Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment

The bioactive CaTiO3 film was grown on the surface of the microwave sintered porous Ti–15Mo alloy by one-step hydrothermal process in supersaturated Ca(OH)2 solution. The microstructures of the film and apatite-forming ability and cytocompatibility of the hydrothermally treated porous Ti–15Mo alloy...

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Main Authors: Lai, T., Xu, J. L., Cao, Xun, Bao, L. Z., Luo, J. M., Huang, Yizhong
Other Authors: School of Materials Science and Engineering
Format: Journal Article
Language:English
Published: 2021
Subjects:
Online Access:https://hdl.handle.net/10356/153916
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author Lai, T.
Xu, J. L.
Cao, Xun
Bao, L. Z.
Luo, J. M.
Huang, Yizhong
author2 School of Materials Science and Engineering
author_facet School of Materials Science and Engineering
Lai, T.
Xu, J. L.
Cao, Xun
Bao, L. Z.
Luo, J. M.
Huang, Yizhong
author_sort Lai, T.
collection NTU
description The bioactive CaTiO3 film was grown on the surface of the microwave sintered porous Ti–15Mo alloy by one-step hydrothermal process in supersaturated Ca(OH)2 solution. The microstructures of the film and apatite-forming ability and cytocompatibility of the hydrothermally treated porous Ti–15Mo alloy were then investigated. The results show that the hydrothermally treated sample has a thickness of approximately 250 nm and is mainly composed of CaTiO3 phase with some –OH groups except the α-Ti and β-Ti phases. The porous structure of the Ti–15Mo alloy has no significant change after hydrothermal treatment. When immersed in SBF solution, the hydroxyapatite preferentially nucleates and grows on the inner surface and the pore sites, forming a layer of the calcium-deficient apatite on the surface of the hydrothermally treated porous Ti–15Mo alloy finally. The hydrothermal treatment is demonstrated to facilitate the proliferation of MG-63 cells over the porous Ti–15Mo alloy surface (p < 0.01), and promote the alloy from Grade 1 of non-toxic material to Grade 0.
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spelling ntu-10356/1539162023-07-14T15:53:21Z Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment Lai, T. Xu, J. L. Cao, Xun Bao, L. Z. Luo, J. M. Huang, Yizhong School of Materials Science and Engineering Engineering::Materials Hydrothermal Treatment Apatite-Forming Ability The bioactive CaTiO3 film was grown on the surface of the microwave sintered porous Ti–15Mo alloy by one-step hydrothermal process in supersaturated Ca(OH)2 solution. The microstructures of the film and apatite-forming ability and cytocompatibility of the hydrothermally treated porous Ti–15Mo alloy were then investigated. The results show that the hydrothermally treated sample has a thickness of approximately 250 nm and is mainly composed of CaTiO3 phase with some –OH groups except the α-Ti and β-Ti phases. The porous structure of the Ti–15Mo alloy has no significant change after hydrothermal treatment. When immersed in SBF solution, the hydroxyapatite preferentially nucleates and grows on the inner surface and the pore sites, forming a layer of the calcium-deficient apatite on the surface of the hydrothermally treated porous Ti–15Mo alloy finally. The hydrothermal treatment is demonstrated to facilitate the proliferation of MG-63 cells over the porous Ti–15Mo alloy surface (p < 0.01), and promote the alloy from Grade 1 of non-toxic material to Grade 0. Published version This work was funded by the National Natural Science Foun-dation of China (51101085, 51764041 and 51704167), the Natural Science Foundation of Jiangxi Province (20202ACBL214011),the Opening Project of National Engineering Research Center for Powder Metallurgy of Titanium & Rare Metals, China (2019004) and the Postgraduate Innovation Special Fund of Nanchang Hangkong University (YC2020-008). 2021-12-16T09:06:21Z 2021-12-16T09:06:21Z 2021 Journal Article Lai, T., Xu, J. L., Cao, X., Bao, L. Z., Luo, J. M. & Huang, Y. (2021). Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment. Journal of Materials Research and Technology, 14, 202-209. https://dx.doi.org/10.1016/j.jmrt.2021.06.065 2238-7854 https://hdl.handle.net/10356/153916 10.1016/j.jmrt.2021.06.065 2-s2.0-85109176635 14 202 209 en Journal of Materials Research and Technology ©2021 The Author(s). Published by Elsevier B.V. This is an open access article under the CCBY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). application/pdf
spellingShingle Engineering::Materials
Hydrothermal Treatment
Apatite-Forming Ability
Lai, T.
Xu, J. L.
Cao, Xun
Bao, L. Z.
Luo, J. M.
Huang, Yizhong
Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment
title Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment
title_full Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment
title_fullStr Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment
title_full_unstemmed Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment
title_short Bioactive CaTiO₃ film prepared on the biomedical porous Ti-15Mo alloy by one-step hydrothermal treatment
title_sort bioactive catio₃ film prepared on the biomedical porous ti 15mo alloy by one step hydrothermal treatment
topic Engineering::Materials
Hydrothermal Treatment
Apatite-Forming Ability
url https://hdl.handle.net/10356/153916
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