High-throughput electrospinning of eco-friendly starch-based nanofibers

Sustainable material has gained attention throughout the years due to its potential as alternative material to mitigate environmental effects brought forth by conventional polymers. There are many approaches to sustainable material fabrication, one of which is electrospinning. Past studies were focu...

Full description

Bibliographic Details
Main Author: Tan, Shane Ching Sian
Other Authors: Hu Xiao
Format: Final Year Project (FYP)
Language:English
Published: Nanyang Technological University 2022
Subjects:
Online Access:https://hdl.handle.net/10356/157086
_version_ 1811693563011923968
author Tan, Shane Ching Sian
author2 Hu Xiao
author_facet Hu Xiao
Tan, Shane Ching Sian
author_sort Tan, Shane Ching Sian
collection NTU
description Sustainable material has gained attention throughout the years due to its potential as alternative material to mitigate environmental effects brought forth by conventional polymers. There are many approaches to sustainable material fabrication, one of which is electrospinning. Past studies were focused on the fabrication from the conventional method of production. Hence, this study seeks to explore the scalability of starch-based nanofibers using wire electrospinning. Fibers of different compositions of native potato starch and pullulan were electrospun. Various parameters were investigated to examine their influence on the resultant fiber morphology and the yield of the fabrication. Solution parameters (polymer concentration, viscosity, and electrical conductivity), process parameters (applied voltage and carriage speed) and ambient parameter (humidity) were investigated for their effects on the resultant fiber morphology and yield. Polymer concentrations, applied voltage and humidity were identified as factors that influences yield of fiber with humidity being the most significant. Fiber diameter increased with increase in starch and pullulan concentration while increase in applied voltage led to reduction in fiber diameter. Additionally, increased pullulan loading was shown to reduce the likelihood of beading in the fabricated fiber mat sample. Infrared spectroscopy showed that the composite fibers have similar spectral features of both starch and pullulan. Thermal analysis of the composite fibers showed intermediate thermal stability when compared to pure starch and pullulan. Mechanical testing was also performed on selected compositions of composite fiber mat samples to compare the mechanical properties. The composite material could find potential use in fields such as biomedical industries when designing new products.
first_indexed 2024-10-01T06:53:40Z
format Final Year Project (FYP)
id ntu-10356/157086
institution Nanyang Technological University
language English
last_indexed 2024-10-01T06:53:40Z
publishDate 2022
publisher Nanyang Technological University
record_format dspace
spelling ntu-10356/1570862022-05-08T13:12:40Z High-throughput electrospinning of eco-friendly starch-based nanofibers Tan, Shane Ching Sian Hu Xiao School of Materials Science and Engineering ASXHU@ntu.edu.sg Engineering::Materials Sustainable material has gained attention throughout the years due to its potential as alternative material to mitigate environmental effects brought forth by conventional polymers. There are many approaches to sustainable material fabrication, one of which is electrospinning. Past studies were focused on the fabrication from the conventional method of production. Hence, this study seeks to explore the scalability of starch-based nanofibers using wire electrospinning. Fibers of different compositions of native potato starch and pullulan were electrospun. Various parameters were investigated to examine their influence on the resultant fiber morphology and the yield of the fabrication. Solution parameters (polymer concentration, viscosity, and electrical conductivity), process parameters (applied voltage and carriage speed) and ambient parameter (humidity) were investigated for their effects on the resultant fiber morphology and yield. Polymer concentrations, applied voltage and humidity were identified as factors that influences yield of fiber with humidity being the most significant. Fiber diameter increased with increase in starch and pullulan concentration while increase in applied voltage led to reduction in fiber diameter. Additionally, increased pullulan loading was shown to reduce the likelihood of beading in the fabricated fiber mat sample. Infrared spectroscopy showed that the composite fibers have similar spectral features of both starch and pullulan. Thermal analysis of the composite fibers showed intermediate thermal stability when compared to pure starch and pullulan. Mechanical testing was also performed on selected compositions of composite fiber mat samples to compare the mechanical properties. The composite material could find potential use in fields such as biomedical industries when designing new products. Bachelor of Engineering (Materials Engineering) 2022-05-08T13:12:40Z 2022-05-08T13:12:40Z 2022 Final Year Project (FYP) Tan, S. C. S. (2022). High-throughput electrospinning of eco-friendly starch-based nanofibers. Final Year Project (FYP), Nanyang Technological University, Singapore. https://hdl.handle.net/10356/157086 https://hdl.handle.net/10356/157086 en application/pdf Nanyang Technological University
spellingShingle Engineering::Materials
Tan, Shane Ching Sian
High-throughput electrospinning of eco-friendly starch-based nanofibers
title High-throughput electrospinning of eco-friendly starch-based nanofibers
title_full High-throughput electrospinning of eco-friendly starch-based nanofibers
title_fullStr High-throughput electrospinning of eco-friendly starch-based nanofibers
title_full_unstemmed High-throughput electrospinning of eco-friendly starch-based nanofibers
title_short High-throughput electrospinning of eco-friendly starch-based nanofibers
title_sort high throughput electrospinning of eco friendly starch based nanofibers
topic Engineering::Materials
url https://hdl.handle.net/10356/157086
work_keys_str_mv AT tanshanechingsian highthroughputelectrospinningofecofriendlystarchbasednanofibers