Graphitisation of waste carbon powder with femtosecond laser annealing

Graphitisation of structural characteristics and improvement in electrical conductivity was reported onto waste carbon powder through femtosecond laser annealing. Raman spectroscopy on the carbon powder pre- and post-annealing showed a shift from amorphous-like carbon to graphitic-like carbon, which...

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Main Authors: Lum, Lucas, Tan, Chong Wei, Siah, Chun Fei, Liang, Kun, Tay, Beng Kang
Other Authors: School of Electrical and Electronic Engineering
Format: Journal Article
Language:English
Published: 2022
Subjects:
Online Access:https://hdl.handle.net/10356/160538
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author Lum, Lucas
Tan, Chong Wei
Siah, Chun Fei
Liang, Kun
Tay, Beng Kang
author2 School of Electrical and Electronic Engineering
author_facet School of Electrical and Electronic Engineering
Lum, Lucas
Tan, Chong Wei
Siah, Chun Fei
Liang, Kun
Tay, Beng Kang
author_sort Lum, Lucas
collection NTU
description Graphitisation of structural characteristics and improvement in electrical conductivity was reported onto waste carbon powder through femtosecond laser annealing. Raman spectroscopy on the carbon powder pre- and post-annealing showed a shift from amorphous-like carbon to graphitic-like carbon, which can be explained by the three-stage model. Electrical I-V probing of the samples revealed an increase in conductivity by up to 90%. An increase in incident laser power was found to be correlated to an increase in conductivity. An average incident laser power of 0.104 W or less showed little to no change in electrical characteristics, while an average incident laser power of greater than 1.626 W had a destructive effect on the carbon powder, shown through the reduction in powder. The most significant improvement in electrical conductivity has been observed at laser powers ranging from 0.526 to 1.286 W. To conclude, the graphitisation of waste carbon powder is possible using post-process femtosecond laser annealing to alter its electrical conductivity for future applications.
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spelling ntu-10356/1605382022-07-26T07:01:09Z Graphitisation of waste carbon powder with femtosecond laser annealing Lum, Lucas Tan, Chong Wei Siah, Chun Fei Liang, Kun Tay, Beng Kang School of Electrical and Electronic Engineering Centre for Micro-/Nano-electronics (NOVITAS) CNRS International NTU THALES Research Alliances Engineering::Electrical and electronic engineering Carbon Black Femtosecond Laser Annealing Graphitisation of structural characteristics and improvement in electrical conductivity was reported onto waste carbon powder through femtosecond laser annealing. Raman spectroscopy on the carbon powder pre- and post-annealing showed a shift from amorphous-like carbon to graphitic-like carbon, which can be explained by the three-stage model. Electrical I-V probing of the samples revealed an increase in conductivity by up to 90%. An increase in incident laser power was found to be correlated to an increase in conductivity. An average incident laser power of 0.104 W or less showed little to no change in electrical characteristics, while an average incident laser power of greater than 1.626 W had a destructive effect on the carbon powder, shown through the reduction in powder. The most significant improvement in electrical conductivity has been observed at laser powers ranging from 0.526 to 1.286 W. To conclude, the graphitisation of waste carbon powder is possible using post-process femtosecond laser annealing to alter its electrical conductivity for future applications. Economic Development Board (EDB) Ministry of Education (MOE) Published version This research was funded by Singapore MOE Tier 2, MOE2018-T2-2-105 and Excelitas Technologies Singapore (EDB-IPP). 2022-07-26T07:01:08Z 2022-07-26T07:01:08Z 2022 Journal Article Lum, L., Tan, C. W., Siah, C. F., Liang, K. & Tay, B. K. (2022). Graphitisation of waste carbon powder with femtosecond laser annealing. Micromachines, 13(1), 120-. https://dx.doi.org/10.3390/mi13010120 2072-666X https://hdl.handle.net/10356/160538 10.3390/mi13010120 35056285 2-s2.0-85123056163 1 13 120 en MOE2018-T2-2-105 EDB-IPP Micromachines © 2022 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). application/pdf
spellingShingle Engineering::Electrical and electronic engineering
Carbon Black
Femtosecond Laser Annealing
Lum, Lucas
Tan, Chong Wei
Siah, Chun Fei
Liang, Kun
Tay, Beng Kang
Graphitisation of waste carbon powder with femtosecond laser annealing
title Graphitisation of waste carbon powder with femtosecond laser annealing
title_full Graphitisation of waste carbon powder with femtosecond laser annealing
title_fullStr Graphitisation of waste carbon powder with femtosecond laser annealing
title_full_unstemmed Graphitisation of waste carbon powder with femtosecond laser annealing
title_short Graphitisation of waste carbon powder with femtosecond laser annealing
title_sort graphitisation of waste carbon powder with femtosecond laser annealing
topic Engineering::Electrical and electronic engineering
Carbon Black
Femtosecond Laser Annealing
url https://hdl.handle.net/10356/160538
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AT siahchunfei graphitisationofwastecarbonpowderwithfemtosecondlaserannealing
AT liangkun graphitisationofwastecarbonpowderwithfemtosecondlaserannealing
AT taybengkang graphitisationofwastecarbonpowderwithfemtosecondlaserannealing