The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion

Owing to the rapid cooling rates and directional thermal gradients involved, fusion-based additive manufacturing (AM) processes yield complex, fine solidification structures that impart anisotropic mechanical properties in materials, such as stainless steel 316L (SS316L). In this work, we present a...

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Main Authors: Tekumalla, Sravya, Selvarajou, Balaji, Raman, Sudharshan, Gao, Shubo, Seita, Matteo
Other Authors: School of Mechanical and Aerospace Engineering
Format: Journal Article
Language:English
Published: 2022
Subjects:
Online Access:https://hdl.handle.net/10356/162001
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author Tekumalla, Sravya
Selvarajou, Balaji
Raman, Sudharshan
Gao, Shubo
Seita, Matteo
author2 School of Mechanical and Aerospace Engineering
author_facet School of Mechanical and Aerospace Engineering
Tekumalla, Sravya
Selvarajou, Balaji
Raman, Sudharshan
Gao, Shubo
Seita, Matteo
author_sort Tekumalla, Sravya
collection NTU
description Owing to the rapid cooling rates and directional thermal gradients involved, fusion-based additive manufacturing (AM) processes yield complex, fine solidification structures that impart anisotropic mechanical properties in materials, such as stainless steel 316L (SS316L). In this work, we present a comprehensive study of the mechanical anisotropy of SS316L produced by laser powder bed fusion using instrumented nanoindentation. We produce and test near-single crystal samples oriented along the three principal crystallographic axes—namely ⟨100⟩, ⟨110⟩, and ⟨111⟩—using a Berkovich indenter. We find that the ⟨111⟩ and ⟨100⟩ orientations exhibit the highest and the lowest hardness, respectively. To decouple the contributions of grain orientation and solidification structure to the alloy's mechanical anisotropy, we compare our experimental results against crystal plasticity finite element (CPFE) simulations. We ascribe the hardness anisotropy in SS316L to the cell spacing along the slip direction (CSSD), which is a novel metric that we introduce to account for the role of the solidification structure on plasticity. Our work provides a universal pathway to understanding the microstructure-property relationships in cubic metallic materials that exhibit solidification structures,such as those commonly imparted by fusion-based AM.
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spelling ntu-10356/1620012022-10-01T23:31:38Z The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion Tekumalla, Sravya Selvarajou, Balaji Raman, Sudharshan Gao, Shubo Seita, Matteo School of Mechanical and Aerospace Engineering School of Materials Science and Engineering Singapore Centre for 3D Printing Engineering::Materials Engineering::Mechanical engineering Laser Powder Bed Fusion Anisotropy Owing to the rapid cooling rates and directional thermal gradients involved, fusion-based additive manufacturing (AM) processes yield complex, fine solidification structures that impart anisotropic mechanical properties in materials, such as stainless steel 316L (SS316L). In this work, we present a comprehensive study of the mechanical anisotropy of SS316L produced by laser powder bed fusion using instrumented nanoindentation. We produce and test near-single crystal samples oriented along the three principal crystallographic axes—namely ⟨100⟩, ⟨110⟩, and ⟨111⟩—using a Berkovich indenter. We find that the ⟨111⟩ and ⟨100⟩ orientations exhibit the highest and the lowest hardness, respectively. To decouple the contributions of grain orientation and solidification structure to the alloy's mechanical anisotropy, we compare our experimental results against crystal plasticity finite element (CPFE) simulations. We ascribe the hardness anisotropy in SS316L to the cell spacing along the slip direction (CSSD), which is a novel metric that we introduce to account for the role of the solidification structure on plasticity. Our work provides a universal pathway to understanding the microstructure-property relationships in cubic metallic materials that exhibit solidification structures,such as those commonly imparted by fusion-based AM. Agency for Science, Technology and Research (A*STAR) Nanyang Technological University National Research Foundation (NRF) Published version This work was supported by the NTU Presidential Postdoctoral Fellowship (Grant number: 04INS000761C160), National Research Foundation (NRF) Singapore, under the NRF Fellowship program (NRF-NRFF2018-05), and A*STAR, Singapore under the Structural Metals and Alloys Program (Grant number: A18B1b0061). 2022-09-28T08:14:32Z 2022-09-28T08:14:32Z 2022 Journal Article Tekumalla, S., Selvarajou, B., Raman, S., Gao, S. & Seita, M. (2022). The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion. Materials Science and Engineering A, 833, 142493-. https://dx.doi.org/10.1016/j.msea.2021.142493 0921-5093 https://hdl.handle.net/10356/162001 10.1016/j.msea.2021.142493 2-s2.0-85122059506 833 142493 en 04INS000761C160 NRF-NRFF2018-05 A18B1b0061 Materials Science and Engineering A © 2021 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). application/pdf
spellingShingle Engineering::Materials
Engineering::Mechanical engineering
Laser Powder Bed Fusion
Anisotropy
Tekumalla, Sravya
Selvarajou, Balaji
Raman, Sudharshan
Gao, Shubo
Seita, Matteo
The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion
title The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion
title_full The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion
title_fullStr The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion
title_full_unstemmed The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion
title_short The role of the solidification structure on orientation-dependent hardness in stainless steel 316L produced by laser powder bed fusion
title_sort role of the solidification structure on orientation dependent hardness in stainless steel 316l produced by laser powder bed fusion
topic Engineering::Materials
Engineering::Mechanical engineering
Laser Powder Bed Fusion
Anisotropy
url https://hdl.handle.net/10356/162001
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