Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings

The current work investigates the successful preparation of Ni-TiN coatings via the jet electrodeposition method. The x-ray diffraction, high-resolution transmission electron microscopy, electrochemical workstation, and triboindenter were used to analyze the structure, mechanical deformation respons...

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Main Authors: Li, Qiang, Xia, Fafeng, Liu, Guifen, Yao, Liming
Andre forfattere: School of Mechanical and Aerospace Engineering
Format: Journal Article
Sprog:English
Udgivet: 2022
Fag:
Online adgang:https://hdl.handle.net/10356/162133
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author Li, Qiang
Xia, Fafeng
Liu, Guifen
Yao, Liming
author2 School of Mechanical and Aerospace Engineering
author_facet School of Mechanical and Aerospace Engineering
Li, Qiang
Xia, Fafeng
Liu, Guifen
Yao, Liming
author_sort Li, Qiang
collection NTU
description The current work investigates the successful preparation of Ni-TiN coatings via the jet electrodeposition method. The x-ray diffraction, high-resolution transmission electron microscopy, electrochemical workstation, and triboindenter were used to analyze the structure, mechanical deformation response, and corrosion properties of the coatings. The results reveal that the Ni-TiN coating produced by the deposition method had a fine and uniform microstructure at a 5 g/L concentration of TiN. The mean sizes of TiN nanoparticles and Ni grains were found to be 23.3 and 43.9 nm, respectively. The corrosion potential of the Ni-based TiN coating obtained at 5 g/L by electrodeposition was as minimum as − 0.396 V with a corrosion current density of 1.06 × 10−3 mA/cm2. The Ni-TiN coatings prepared, respectively, at three different concentrations (3, 5, and 8 g/L) under the applied load of 1500 µN were about 34.9, 28.2, and 30.3 µm in vertical depth, respectively. The coatings obtained at 5 g/L had the maximum nanohardness of 34.5 GPa when compared to the other coatings. In addition, the coatings were then subjected to three sliding scans, and the Ni-TiN coating prepared at 5 g/L showed the least magnitude of wear damage and plastic deformation when compared to the other coatings.
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spelling ntu-10356/1621332022-10-05T01:53:03Z Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings Li, Qiang Xia, Fafeng Liu, Guifen Yao, Liming School of Mechanical and Aerospace Engineering Engineering::Mechanical engineering Coating Jet Electrodeposition The current work investigates the successful preparation of Ni-TiN coatings via the jet electrodeposition method. The x-ray diffraction, high-resolution transmission electron microscopy, electrochemical workstation, and triboindenter were used to analyze the structure, mechanical deformation response, and corrosion properties of the coatings. The results reveal that the Ni-TiN coating produced by the deposition method had a fine and uniform microstructure at a 5 g/L concentration of TiN. The mean sizes of TiN nanoparticles and Ni grains were found to be 23.3 and 43.9 nm, respectively. The corrosion potential of the Ni-based TiN coating obtained at 5 g/L by electrodeposition was as minimum as − 0.396 V with a corrosion current density of 1.06 × 10−3 mA/cm2. The Ni-TiN coatings prepared, respectively, at three different concentrations (3, 5, and 8 g/L) under the applied load of 1500 µN were about 34.9, 28.2, and 30.3 µm in vertical depth, respectively. The coatings obtained at 5 g/L had the maximum nanohardness of 34.5 GPa when compared to the other coatings. In addition, the coatings were then subjected to three sliding scans, and the Ni-TiN coating prepared at 5 g/L showed the least magnitude of wear damage and plastic deformation when compared to the other coatings. This work has been supported by the Natural Science Foundation of China (Grant No. 51974089). 2022-10-05T01:53:03Z 2022-10-05T01:53:03Z 2022 Journal Article Li, Q., Xia, F., Liu, G. & Yao, L. (2022). Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings. Journal of Materials Engineering and Performance. https://dx.doi.org/10.1007/s11665-022-06909-y 1059-9495 https://hdl.handle.net/10356/162133 10.1007/s11665-022-06909-y 2-s2.0-85129238903 en Journal of Materials Engineering and Performance © 2022 ASM International. All rights reserved.
spellingShingle Engineering::Mechanical engineering
Coating
Jet Electrodeposition
Li, Qiang
Xia, Fafeng
Liu, Guifen
Yao, Liming
Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings
title Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings
title_full Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings
title_fullStr Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings
title_full_unstemmed Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings
title_short Microstructure and properties of jet pulse electrodeposited Ni-TiN nanocoatings
title_sort microstructure and properties of jet pulse electrodeposited ni tin nanocoatings
topic Engineering::Mechanical engineering
Coating
Jet Electrodeposition
url https://hdl.handle.net/10356/162133
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AT xiafafeng microstructureandpropertiesofjetpulseelectrodepositednitinnanocoatings
AT liuguifen microstructureandpropertiesofjetpulseelectrodepositednitinnanocoatings
AT yaoliming microstructureandpropertiesofjetpulseelectrodepositednitinnanocoatings