A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys

Recrystallization, possibly triggered during heat treatments by plastic strains of only 1–2%, is highly deleterious to Ni-based single-crystal superalloys. Herein, we successfully recover plastic deformation and enhance the supersolvus critical strain for recrystallization by ramping the annealing t...

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Main Authors: Lin, Sicong, Chen, Kai, Zeng, Qiang, Ramamurty, Upadrasta
Other Authors: School of Mechanical and Aerospace Engineering
Format: Journal Article
Language:English
Published: 2023
Subjects:
Online Access:https://hdl.handle.net/10356/171571
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author Lin, Sicong
Chen, Kai
Zeng, Qiang
Ramamurty, Upadrasta
author2 School of Mechanical and Aerospace Engineering
author_facet School of Mechanical and Aerospace Engineering
Lin, Sicong
Chen, Kai
Zeng, Qiang
Ramamurty, Upadrasta
author_sort Lin, Sicong
collection NTU
description Recrystallization, possibly triggered during heat treatments by plastic strains of only 1–2%, is highly deleterious to Ni-based single-crystal superalloys. Herein, we successfully recover plastic deformation and enhance the supersolvus critical strain for recrystallization by ramping the annealing temperature slowly from 1100 °C to γ′-solvus point. This preempts recrystallization during the subsequent supersolvus solutionizing treatment. The proposed method is validated in single-crystals compressed to 5.9% plastic strain at room temperature. After supersolvus solutionizing, an almost dislocation-free single-crystal with uniformly distributed γ′-precipitates is obtained. The proposed method offers a practical means to bring down the overall expenses of single-crystal turbine blades.
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spelling ntu-10356/1715712023-11-04T16:48:10Z A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys Lin, Sicong Chen, Kai Zeng, Qiang Ramamurty, Upadrasta School of Mechanical and Aerospace Engineering Institute of Material Research and Engineering, A*STAR Engineering::Materials Recovery Heat Treatment Recrystallization Critical Strain Recrystallization, possibly triggered during heat treatments by plastic strains of only 1–2%, is highly deleterious to Ni-based single-crystal superalloys. Herein, we successfully recover plastic deformation and enhance the supersolvus critical strain for recrystallization by ramping the annealing temperature slowly from 1100 °C to γ′-solvus point. This preempts recrystallization during the subsequent supersolvus solutionizing treatment. The proposed method is validated in single-crystals compressed to 5.9% plastic strain at room temperature. After supersolvus solutionizing, an almost dislocation-free single-crystal with uniformly distributed γ′-precipitates is obtained. The proposed method offers a practical means to bring down the overall expenses of single-crystal turbine blades. Published version This work was supported by National Science and Technology Major Project: [Grant Number 2019-VII-0019-0161]; National Natural Science Foundation of China: [Grant Number 51927801, U2032205, and 52271042]; Outstanding Young Scholar Program: [Grant Number 2020-JCJQ-009]; 111 Project 2.0: [Grant Number BP0618008]. 2023-10-31T02:29:37Z 2023-10-31T02:29:37Z 2023 Journal Article Lin, S., Chen, K., Zeng, Q. & Ramamurty, U. (2023). A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys. Materials Research Letters, 11(10), 856-862. https://dx.doi.org/10.1080/21663831.2023.2253267 2166-3831 https://hdl.handle.net/10356/171571 10.1080/21663831.2023.2253267 2-s2.0-85169664667 10 11 856 862 en Materials Research Letters © 2023 The Author(s). Published by Informa UK Limited, trading as Taylor & Francis Group. This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The terms on which this article has been published allow the posting of the Accepted Manuscript in a repository by the author(s) or with their consent. application/pdf
spellingShingle Engineering::Materials
Recovery Heat Treatment
Recrystallization Critical Strain
Lin, Sicong
Chen, Kai
Zeng, Qiang
Ramamurty, Upadrasta
A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys
title A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys
title_full A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys
title_fullStr A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys
title_full_unstemmed A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys
title_short A method for increasing the supersolvus critical strain for recrystallization in single-crystal superalloys
title_sort method for increasing the supersolvus critical strain for recrystallization in single crystal superalloys
topic Engineering::Materials
Recovery Heat Treatment
Recrystallization Critical Strain
url https://hdl.handle.net/10356/171571
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