Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater
The project aim is to study the pairing of TiO2 nanotubes and FeCo nanoparticles as a novel treatment method to remove fluoride content from semiconductor wastewater. The research is split into two papers – Si Yuan’s FYP report and this report. This report covers the synthesis of TiO2 nanotubes usin...
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| Format: | Final Year Project (FYP) |
| Language: | English |
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Nanyang Technological University
2023
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| Online Access: | https://hdl.handle.net/10356/172522 |
| _version_ | 1824453672425226240 |
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| author | Yap, Brendan Ee Herng |
| author2 | Darren Sun Delai |
| author_facet | Darren Sun Delai Yap, Brendan Ee Herng |
| author_sort | Yap, Brendan Ee Herng |
| collection | NTU |
| description | The project aim is to study the pairing of TiO2 nanotubes and FeCo nanoparticles as a novel treatment method to remove fluoride content from semiconductor wastewater. The research is split into two papers – Si Yuan’s FYP report and this report. This report covers the synthesis of TiO2 nanotubes using the sonicated hydrothermal process, and the synthesis of FeCo nanoparticles using coprecipitation. TiO2 nanotubes synthesised via the sonication hydrothermal method showed a significant increase in length of nanotube due to effects of sonication. However, energy dispersive X-ray (EDX) and X-ray diffraction (XRD) showed the presence of Na in sample B1 and is assumed to have caused a reduction in length of nanotube. FeCo nanoparticles were synthesised using the coprecipitation method with ferric chloride and cobalt nitrate hexahydrate as precursors in the presence of ethanol glycol as dispersant. A total of two batches were synthesised with one having higher Fe concentrations (120723) and vice versa. It was observed that the batch (090723) with lower Fe concentrations displayed no magnetic properties. FESEM results revealed successful synthesis of the nanoparticles coated with the nanotubes, EDX and XRD results revealed that the nanoparticles were of low purity due to presence of impurities that were not properly removed during synthesis. The synthesis method needs to be reviewed again to remove/reduce the impurities present. |
| first_indexed | 2025-02-19T03:10:08Z |
| format | Final Year Project (FYP) |
| id | ntu-10356/172522 |
| institution | Nanyang Technological University |
| language | English |
| last_indexed | 2025-02-19T03:10:08Z |
| publishDate | 2023 |
| publisher | Nanyang Technological University |
| record_format | dspace |
| spelling | ntu-10356/1725222023-12-15T15:35:03Z Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater Yap, Brendan Ee Herng Darren Sun Delai School of Civil and Environmental Engineering DDSun@ntu.edu.sg Engineering::Environmental engineering::Water treatment The project aim is to study the pairing of TiO2 nanotubes and FeCo nanoparticles as a novel treatment method to remove fluoride content from semiconductor wastewater. The research is split into two papers – Si Yuan’s FYP report and this report. This report covers the synthesis of TiO2 nanotubes using the sonicated hydrothermal process, and the synthesis of FeCo nanoparticles using coprecipitation. TiO2 nanotubes synthesised via the sonication hydrothermal method showed a significant increase in length of nanotube due to effects of sonication. However, energy dispersive X-ray (EDX) and X-ray diffraction (XRD) showed the presence of Na in sample B1 and is assumed to have caused a reduction in length of nanotube. FeCo nanoparticles were synthesised using the coprecipitation method with ferric chloride and cobalt nitrate hexahydrate as precursors in the presence of ethanol glycol as dispersant. A total of two batches were synthesised with one having higher Fe concentrations (120723) and vice versa. It was observed that the batch (090723) with lower Fe concentrations displayed no magnetic properties. FESEM results revealed successful synthesis of the nanoparticles coated with the nanotubes, EDX and XRD results revealed that the nanoparticles were of low purity due to presence of impurities that were not properly removed during synthesis. The synthesis method needs to be reviewed again to remove/reduce the impurities present. Bachelor of Engineering (Environmental Engineering) 2023-12-13T08:20:31Z 2023-12-13T08:20:31Z 2023 Final Year Project (FYP) Yap, B. E. H. (2023). Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater. Final Year Project (FYP), Nanyang Technological University, Singapore. https://hdl.handle.net/10356/172522 https://hdl.handle.net/10356/172522 en application/pdf Nanyang Technological University |
| spellingShingle | Engineering::Environmental engineering::Water treatment Yap, Brendan Ee Herng Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater |
| title | Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater |
| title_full | Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater |
| title_fullStr | Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater |
| title_full_unstemmed | Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater |
| title_short | Synthesis of TiO2/FeCo magnetic nanoparticles as a nano-coagulant for removal of fluoride in semiconductor wastewater |
| title_sort | synthesis of tio2 feco magnetic nanoparticles as a nano coagulant for removal of fluoride in semiconductor wastewater |
| topic | Engineering::Environmental engineering::Water treatment |
| url | https://hdl.handle.net/10356/172522 |
| work_keys_str_mv | AT yapbrendaneeherng synthesisoftio2fecomagneticnanoparticlesasananocoagulantforremovaloffluorideinsemiconductorwastewater |