Deposition of Magneli TiOx on Ti substrate for electroxidation in water treatment

This projectfocuses on the fabrication of Magnéli Phased Titanium sub-oxides coated Titanium electrode for electrochemical application. Two different methods of depositing Magnéli Phased Titanium sub-oxides on Titanium substrates were studied. Method I employed the idea of coating of TiO2 sol-...

Ամբողջական նկարագրություն

Մատենագիտական մանրամասներ
Հիմնական հեղինակ: Lee, Wei Han.
Այլ հեղինակներ: Long Yi
Ձևաչափ: Final Year Project (FYP)
Լեզու:English
Հրապարակվել է: 2013
Խորագրեր:
Առցանց հասանելիություն:http://hdl.handle.net/10356/51860
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author Lee, Wei Han.
author2 Long Yi
author_facet Long Yi
Lee, Wei Han.
author_sort Lee, Wei Han.
collection NTU
description This projectfocuses on the fabrication of Magnéli Phased Titanium sub-oxides coated Titanium electrode for electrochemical application. Two different methods of depositing Magnéli Phased Titanium sub-oxides on Titanium substrates were studied. Method I employed the idea of coating of TiO2 sol-gel on the substrate and followed by reduction in hydrogen atmosphere to obtain Magnéli Phased Titanium sub - oxides. Method II however started off with reduction of TiO2 powder to Magnéli Phased Titanium sub-oxides powder before coating them onto the substrate with sol. Three different coating methods were also adapted in coating the substrates in Method II; they were spin, dip and roll-to-roll coating. Cyclic voltammetry test was conducted to investigate the electrochemical properties of the electrodes fabricated. Method II exhibited film with better mechanical stability and coverage than Method I’s electrodes. However it showed sign of re-oxidation of Magnéli Phased Titanium sub-oxides. For Method II, the SEM imaging showed that dip and roll-to-roll coating has better coverage of the film with increased porosity than spin coating.
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spelling ntu-10356/518602023-03-04T15:35:00Z Deposition of Magneli TiOx on Ti substrate for electroxidation in water treatment Lee, Wei Han. Long Yi School of Materials Science and Engineering DRNTU::Engineering::Materials This projectfocuses on the fabrication of Magnéli Phased Titanium sub-oxides coated Titanium electrode for electrochemical application. Two different methods of depositing Magnéli Phased Titanium sub-oxides on Titanium substrates were studied. Method I employed the idea of coating of TiO2 sol-gel on the substrate and followed by reduction in hydrogen atmosphere to obtain Magnéli Phased Titanium sub - oxides. Method II however started off with reduction of TiO2 powder to Magnéli Phased Titanium sub-oxides powder before coating them onto the substrate with sol. Three different coating methods were also adapted in coating the substrates in Method II; they were spin, dip and roll-to-roll coating. Cyclic voltammetry test was conducted to investigate the electrochemical properties of the electrodes fabricated. Method II exhibited film with better mechanical stability and coverage than Method I’s electrodes. However it showed sign of re-oxidation of Magnéli Phased Titanium sub-oxides. For Method II, the SEM imaging showed that dip and roll-to-roll coating has better coverage of the film with increased porosity than spin coating. Bachelor of Engineering (Materials Engineering) 2013-04-11T08:18:36Z 2013-04-11T08:18:36Z 2013 2013 Final Year Project (FYP) http://hdl.handle.net/10356/51860 en Nanyang Technological University 50 p. application/pdf
spellingShingle DRNTU::Engineering::Materials
Lee, Wei Han.
Deposition of Magneli TiOx on Ti substrate for electroxidation in water treatment
title Deposition of Magneli TiOx on Ti substrate for electroxidation in water treatment
title_full Deposition of Magneli TiOx on Ti substrate for electroxidation in water treatment
title_fullStr Deposition of Magneli TiOx on Ti substrate for electroxidation in water treatment
title_full_unstemmed Deposition of Magneli TiOx on Ti substrate for electroxidation in water treatment
title_short Deposition of Magneli TiOx on Ti substrate for electroxidation in water treatment
title_sort deposition of magneli tiox on ti substrate for electroxidation in water treatment
topic DRNTU::Engineering::Materials
url http://hdl.handle.net/10356/51860
work_keys_str_mv AT leeweihan depositionofmagnelitioxontisubstrateforelectroxidationinwatertreatment