A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals

Practical, efficient synthesis of metal oxide nanocrystals with good crystallinity and high specific surface area by a modified polymer-network gel method is demonstrated, taking ZnO nanocrystals as an example. A novel stepwise heat treatment yields significant improvement in crystal quality. Such n...

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Main Authors: Xu, Shuyan, Xiong, G., Zhang, Q. P., Xu, X. N., Liu, Y. T., Xu, M., Deng, S. H., Chen, Y., Yuan, H., Yu, F., Huang, Y., Zhao, K.
Other Authors: Institute of Advanced Studies
Format: Journal Article
Language:English
Published: 2018
Subjects:
Online Access:https://hdl.handle.net/10356/89606
http://hdl.handle.net/10220/44989
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author Xu, Shuyan
Xiong, G.
Zhang, Q. P.
Xu, X. N.
Liu, Y. T.
Xu, M.
Deng, S. H.
Chen, Y.
Yuan, H.
Yu, F.
Huang, Y.
Zhao, K.
author2 Institute of Advanced Studies
author_facet Institute of Advanced Studies
Xu, Shuyan
Xiong, G.
Zhang, Q. P.
Xu, X. N.
Liu, Y. T.
Xu, M.
Deng, S. H.
Chen, Y.
Yuan, H.
Yu, F.
Huang, Y.
Zhao, K.
author_sort Xu, Shuyan
collection NTU
description Practical, efficient synthesis of metal oxide nanocrystals with good crystallinity and high specific surface area by a modified polymer-network gel method is demonstrated, taking ZnO nanocrystals as an example. A novel stepwise heat treatment yields significant improvement in crystal quality. Such nanophase materials can effectively degrade common organic dyes under solar radiation and can perform very well in photo-assisted detection of NO2 gas. Other typical metal oxide nanocrystals with good crystallinity and high specific surface area were also synthesized successfully under similar conditions. This work provides a general strategy for the synthesis of metal oxide nanocrystals, balancing the crystallinity and specific surface area.
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spelling ntu-10356/896062020-09-26T21:55:58Z A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals Xu, Shuyan Xiong, G. Zhang, Q. P. Xu, X. N. Liu, Y. T. Xu, M. Deng, S. H. Chen, Y. Yuan, H. Yu, F. Huang, Y. Zhao, K. Institute of Advanced Studies Materials for Energy and Catalysis Nanoscale Materials Practical, efficient synthesis of metal oxide nanocrystals with good crystallinity and high specific surface area by a modified polymer-network gel method is demonstrated, taking ZnO nanocrystals as an example. A novel stepwise heat treatment yields significant improvement in crystal quality. Such nanophase materials can effectively degrade common organic dyes under solar radiation and can perform very well in photo-assisted detection of NO2 gas. Other typical metal oxide nanocrystals with good crystallinity and high specific surface area were also synthesized successfully under similar conditions. This work provides a general strategy for the synthesis of metal oxide nanocrystals, balancing the crystallinity and specific surface area. Published version 2018-06-07T07:13:53Z 2019-12-06T17:29:25Z 2018-06-07T07:13:53Z 2019-12-06T17:29:25Z 2017 Journal Article Zhang, Q. P., Xu, X. N., Liu, Y. T., Xu, M., Deng, S. H., Chen, Y., et al. (2017). A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals. Scientific Reports, 7, 46424-. 2045-2322 https://hdl.handle.net/10356/89606 http://hdl.handle.net/10220/44989 10.1038/srep46424 en Scientific Reports © 2017 The Author(s). This work is licensed under a Creative Commons Attribution 4.0 International License. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in the credit line; if the material is not included under the Creative Commons license, users will need to obtain permission from the license holder to reproduce the material. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/ 12 p. application/pdf
spellingShingle Materials for Energy and Catalysis
Nanoscale Materials
Xu, Shuyan
Xiong, G.
Zhang, Q. P.
Xu, X. N.
Liu, Y. T.
Xu, M.
Deng, S. H.
Chen, Y.
Yuan, H.
Yu, F.
Huang, Y.
Zhao, K.
A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals
title A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals
title_full A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals
title_fullStr A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals
title_full_unstemmed A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals
title_short A feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals
title_sort feasible strategy to balance the crystallinity and specific surface area of metal oxide nanocrystals
topic Materials for Energy and Catalysis
Nanoscale Materials
url https://hdl.handle.net/10356/89606
http://hdl.handle.net/10220/44989
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