Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel

A new route to obtain a layer of micro-nanostructured Fe3O4 using hydrothermal method has been reported. The prepared dual-scale film, after a two-stage heat treatment and surface modification with dopamine and octadecylamine, shows a contact angle of 158.3° and sliding angle of 3.3°. The corrosion...

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Main Authors: He, Shijun, Wang, Zhen, Hu, Jun, Zhu, Jianbo, Wei, Liping, Chen, Zhong
Other Authors: School of Materials Science & Engineering
Format: Journal Article
Language:English
Published: 2019
Subjects:
Online Access:https://hdl.handle.net/10356/90057
http://hdl.handle.net/10220/49431
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author He, Shijun
Wang, Zhen
Hu, Jun
Zhu, Jianbo
Wei, Liping
Chen, Zhong
author2 School of Materials Science & Engineering
author_facet School of Materials Science & Engineering
He, Shijun
Wang, Zhen
Hu, Jun
Zhu, Jianbo
Wei, Liping
Chen, Zhong
author_sort He, Shijun
collection NTU
description A new route to obtain a layer of micro-nanostructured Fe3O4 using hydrothermal method has been reported. The prepared dual-scale film, after a two-stage heat treatment and surface modification with dopamine and octadecylamine, shows a contact angle of 158.3° and sliding angle of 3.3°. The corrosion current density and the impedance of the superhydrophobic surface protected steel sample were, respectively, one order of magnitude lower and 32 times higher than that of the bare N80 steel in a 5 wt% NaCl aqueous solution. The superhydrophobic Fe3O4 film demonstrated excellent self-cleaning performance and was able to maintain its anti-wetting performance after water jetting test. Our work finds that annealing in N2 and then in O2 plays a significant role in fabricating the superhydrophobic Fe3O4 film for corrosion protection as this treatment is able to realize the desirable micro-nanostructured oxide structure.
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spelling ntu-10356/900572023-07-14T15:52:44Z Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel He, Shijun Wang, Zhen Hu, Jun Zhu, Jianbo Wei, Liping Chen, Zhong School of Materials Science & Engineering Superhydrophobic Fe3O4 Engineering::Materials A new route to obtain a layer of micro-nanostructured Fe3O4 using hydrothermal method has been reported. The prepared dual-scale film, after a two-stage heat treatment and surface modification with dopamine and octadecylamine, shows a contact angle of 158.3° and sliding angle of 3.3°. The corrosion current density and the impedance of the superhydrophobic surface protected steel sample were, respectively, one order of magnitude lower and 32 times higher than that of the bare N80 steel in a 5 wt% NaCl aqueous solution. The superhydrophobic Fe3O4 film demonstrated excellent self-cleaning performance and was able to maintain its anti-wetting performance after water jetting test. Our work finds that annealing in N2 and then in O2 plays a significant role in fabricating the superhydrophobic Fe3O4 film for corrosion protection as this treatment is able to realize the desirable micro-nanostructured oxide structure. Published version 2019-07-18T07:14:42Z 2019-12-06T17:39:44Z 2019-07-18T07:14:42Z 2019-12-06T17:39:44Z 2018 Journal Article He, S., Wang, Z., Hu, J., Zhu, J., Wei, L., & Chen, Z. (2018). Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel. Materials and Design, 160, 84-94. doi:10.1016/j.matdes.2018.09.002 0261-3069 https://hdl.handle.net/10356/90057 http://hdl.handle.net/10220/49431 10.1016/j.matdes.2018.09.002 en Materials and Design © 2018 Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). 11 p. application/pdf
spellingShingle Superhydrophobic
Fe3O4
Engineering::Materials
He, Shijun
Wang, Zhen
Hu, Jun
Zhu, Jianbo
Wei, Liping
Chen, Zhong
Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel
title Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel
title_full Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel
title_fullStr Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel
title_full_unstemmed Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel
title_short Formation of superhydrophobic micro-nanostructured iron oxide for corrosion protection of N80 steel
title_sort formation of superhydrophobic micro nanostructured iron oxide for corrosion protection of n80 steel
topic Superhydrophobic
Fe3O4
Engineering::Materials
url https://hdl.handle.net/10356/90057
http://hdl.handle.net/10220/49431
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