Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique

In the fabrication of microfluidic devices by hot embossing, secondary molds made from epoxy and other polymeric materials with high Tg are commonly used in lab-scale research and for short production runs of several hundred products. However, few studies have been conducted to compare the performan...

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Main Authors: Gupta, A., Tang, P. S., Jena, Rajeeb Kumar, Yue, Chee Yoon, Lam, Yee Cheong
Other Authors: School of Mechanical and Aerospace Engineering
Format: Journal Article
Language:English
Published: 2013
Subjects:
Online Access:https://hdl.handle.net/10356/97844
http://hdl.handle.net/10220/12099
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author Gupta, A.
Tang, P. S.
Jena, Rajeeb Kumar
Yue, Chee Yoon
Lam, Yee Cheong
author2 School of Mechanical and Aerospace Engineering
author_facet School of Mechanical and Aerospace Engineering
Gupta, A.
Tang, P. S.
Jena, Rajeeb Kumar
Yue, Chee Yoon
Lam, Yee Cheong
author_sort Gupta, A.
collection NTU
description In the fabrication of microfluidic devices by hot embossing, secondary molds made from epoxy and other polymeric materials with high Tg are commonly used in lab-scale research and for short production runs of several hundred products. However, few studies have been conducted to compare the performance and efficacy of such molds compared to the master silicon mold. To allow such molds to be exploited fully, this study investigates the performance of silicon, epoxy and COC (TOPAS-6017 grade) molds to fabricate microchannels on COC (TOPAS-8007 grade) substrate using hot embossing. The degree of filling of the mold cavity during microfabrication was assessed. At the optimum embossing conditions (i.e. 100 °C, 2.94 kN load and 5 min loading time), all three molds had similar performance in terms of replication fidelity. However, at sub-optimum conditions (e.g. 80 °C), the silicon mold was the best in terms of mold cavity filling followed by COC and epoxy. For surface roughness and friction coefficient which are important factors affecting tool life, it was found that epoxy mold gives the lowest values followed by COC and silicon. The surface energy determined using contact angle measurements gave a similar trend with epoxy having the lowest surface energy (28 dyne/cm), followed by COC (33.52 dyne/cm) and silicon (71.63 dynedyne/cm). A lower surface energy will result in lower adhesion and friction coefficient between the polymer and mold, resulting in easier demolding.
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spelling ntu-10356/978442020-03-07T13:22:16Z Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique Gupta, A. Tang, P. S. Jena, Rajeeb Kumar Yue, Chee Yoon Lam, Yee Cheong School of Mechanical and Aerospace Engineering Singapore-MIT Alliance Programme DRNTU::Engineering::Mechanical engineering In the fabrication of microfluidic devices by hot embossing, secondary molds made from epoxy and other polymeric materials with high Tg are commonly used in lab-scale research and for short production runs of several hundred products. However, few studies have been conducted to compare the performance and efficacy of such molds compared to the master silicon mold. To allow such molds to be exploited fully, this study investigates the performance of silicon, epoxy and COC (TOPAS-6017 grade) molds to fabricate microchannels on COC (TOPAS-8007 grade) substrate using hot embossing. The degree of filling of the mold cavity during microfabrication was assessed. At the optimum embossing conditions (i.e. 100 °C, 2.94 kN load and 5 min loading time), all three molds had similar performance in terms of replication fidelity. However, at sub-optimum conditions (e.g. 80 °C), the silicon mold was the best in terms of mold cavity filling followed by COC and epoxy. For surface roughness and friction coefficient which are important factors affecting tool life, it was found that epoxy mold gives the lowest values followed by COC and silicon. The surface energy determined using contact angle measurements gave a similar trend with epoxy having the lowest surface energy (28 dyne/cm), followed by COC (33.52 dyne/cm) and silicon (71.63 dynedyne/cm). A lower surface energy will result in lower adhesion and friction coefficient between the polymer and mold, resulting in easier demolding. 2013-07-24T04:14:05Z 2019-12-06T19:47:18Z 2013-07-24T04:14:05Z 2019-12-06T19:47:18Z 2012 2012 Journal Article Jena, R. K., Yue, C. Y., Lam, Y. C., Tang, P. S., & Gupta, A. (2012). Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique. Sensors and actuators B : chemical, 163(1), 233-241. 0925-4005 https://hdl.handle.net/10356/97844 http://hdl.handle.net/10220/12099 10.1016/j.snb.2012.01.043 en Sensors and actuators B : chemical © 2012 Elsevier B.V.
spellingShingle DRNTU::Engineering::Mechanical engineering
Gupta, A.
Tang, P. S.
Jena, Rajeeb Kumar
Yue, Chee Yoon
Lam, Yee Cheong
Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique
title Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique
title_full Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique
title_fullStr Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique
title_full_unstemmed Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique
title_short Comparison of different molds (epoxy, polymer and silicon) for microfabrication by hot embossing technique
title_sort comparison of different molds epoxy polymer and silicon for microfabrication by hot embossing technique
topic DRNTU::Engineering::Mechanical engineering
url https://hdl.handle.net/10356/97844
http://hdl.handle.net/10220/12099
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