Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions

Magnetic chitosan beads were prepared by 3 different weight ratios of Fe3O4 : chitosan, i.e. 1:1, 5:1 and 10:1, and were cross-linked with glutaraldehyde. Physical characterizations of the beads were carried out by scanning electron microscope (SEM), image analyzer, Fourier transformed infrared spec...

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Main Authors: Mohd Daud, Jamaluddin, Ahmad, Nurliza
Format: Proceeding Paper
Language:English
Published: 2008
Subjects:
Online Access:http://irep.iium.edu.my/12344/1/Poster_Magnetic_Chitosan_NZ_Conference_2008_%21.pdf
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author Mohd Daud, Jamaluddin
Ahmad, Nurliza
author_facet Mohd Daud, Jamaluddin
Ahmad, Nurliza
author_sort Mohd Daud, Jamaluddin
collection IIUM
description Magnetic chitosan beads were prepared by 3 different weight ratios of Fe3O4 : chitosan, i.e. 1:1, 5:1 and 10:1, and were cross-linked with glutaraldehyde. Physical characterizations of the beads were carried out by scanning electron microscope (SEM), image analyzer, Fourier transformed infrared spectrometer (FTIR) and vibrating-sample magnetometer (VSM). The influence of pH, contact time and platinum (IV) ions concentration were studied in order to achieve the optimum adsorption conditions by solid phase extraction (SPE) method of static mode. Recovery of the adsorbed platinum (IV) ions from the beads was carried out by desorption with 1.0 M ammonium thiocyanate solution.
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spelling oai:generic.eprints.org:123442013-07-08T03:34:21Z http://irep.iium.edu.my/12344/ Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions Mohd Daud, Jamaluddin Ahmad, Nurliza QD Chemistry Magnetic chitosan beads were prepared by 3 different weight ratios of Fe3O4 : chitosan, i.e. 1:1, 5:1 and 10:1, and were cross-linked with glutaraldehyde. Physical characterizations of the beads were carried out by scanning electron microscope (SEM), image analyzer, Fourier transformed infrared spectrometer (FTIR) and vibrating-sample magnetometer (VSM). The influence of pH, contact time and platinum (IV) ions concentration were studied in order to achieve the optimum adsorption conditions by solid phase extraction (SPE) method of static mode. Recovery of the adsorbed platinum (IV) ions from the beads was carried out by desorption with 1.0 M ammonium thiocyanate solution. 2008-11-30 Proceeding Paper PeerReviewed application/pdf en http://irep.iium.edu.my/12344/1/Poster_Magnetic_Chitosan_NZ_Conference_2008_%21.pdf Mohd Daud, Jamaluddin and Ahmad, Nurliza (2008) Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions. In: Chemistry and the Biosphere Conference, 30rd Nov - 4th December 2008, University of Otago, Dunedin, New Zealand. http://www.otago.ac.nz/nzic/Postertitles.pdf
spellingShingle QD Chemistry
Mohd Daud, Jamaluddin
Ahmad, Nurliza
Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions
title Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions
title_full Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions
title_fullStr Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions
title_full_unstemmed Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions
title_short Preparation and characterization of magnetic chitosan and its application for preconcentration of platinum(IV) metal ions
title_sort preparation and characterization of magnetic chitosan and its application for preconcentration of platinum iv metal ions
topic QD Chemistry
url http://irep.iium.edu.my/12344/1/Poster_Magnetic_Chitosan_NZ_Conference_2008_%21.pdf
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