VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT)
Analysis technology of pesticide residues more develop in a row with increases usage pesticide in a field. There are several of residues analysis method, one of them is HPLC. This research aims to perform validate posseses of analysis deltamethrin using a Shimadzu 6.1 high-performance liquid chromat...
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| Format: | Thesis |
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[Yogyakarta] : Universitas Gadjah Mada
2014
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| author | , PRADITA RENDYAWAN , drh. R. Gagak Donny Satria, M.P., M.Pd. |
| author_facet | , PRADITA RENDYAWAN , drh. R. Gagak Donny Satria, M.P., M.Pd. |
| author_sort | , PRADITA RENDYAWAN |
| collection | UGM |
| description | Analysis technology of pesticide residues more develop in a row with
increases usage pesticide in a field. There are several of residues analysis method,
one of them is HPLC.
This research aims to perform validate posseses of analysis deltamethrin
using a Shimadzu 6.1 high-performance liquid chromatography (HPLC) with control
system SCL-10 A VP, DGU-14 A degasser. Mobile phase of Merck acetonitrile 80%
in steryl aquadest, flow rate of 1.25 ml/minute, UV-Vis SPD 10 AV VP detector with
wavelength of 236 nm and used Shimadzu Shim-pack 150 L x 4.6 mm VP-ODS
Column C18 on temperature 30 oC. The validation examination is based on
specificity, precision, accuracy, limit of qualitative, quantitative limits, and linearity.
Results of the research shows the average of area concentration 1 μg/ml,
2 μg/ml, and 5 μg/ml in consecutive are 34620.33, 79048.67, dan 181208.7 with
retention time in 8.6-8.98 minute. Repeatability is clone 3 times and the RSD mean
value obtained is � 2%. The detection limit at 0.1 μg/ml and limit of quantification at
concententration 1 μg/ml. The equation of linear line y = 36046x+2182, with the
value of R= 0.99. It can be concluded that the method used in the research posseses
good validity. |
| first_indexed | 2024-03-13T23:32:48Z |
| format | Thesis |
| id | oai:generic.eprints.org:131360 |
| institution | Universiti Gadjah Mada |
| last_indexed | 2024-03-13T23:32:48Z |
| publishDate | 2014 |
| publisher | [Yogyakarta] : Universitas Gadjah Mada |
| record_format | dspace |
| spelling | oai:generic.eprints.org:1313602016-03-04T08:06:27Z https://repository.ugm.ac.id/131360/ VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT) , PRADITA RENDYAWAN , drh. R. Gagak Donny Satria, M.P., M.Pd. ETD Analysis technology of pesticide residues more develop in a row with increases usage pesticide in a field. There are several of residues analysis method, one of them is HPLC. This research aims to perform validate posseses of analysis deltamethrin using a Shimadzu 6.1 high-performance liquid chromatography (HPLC) with control system SCL-10 A VP, DGU-14 A degasser. Mobile phase of Merck acetonitrile 80% in steryl aquadest, flow rate of 1.25 ml/minute, UV-Vis SPD 10 AV VP detector with wavelength of 236 nm and used Shimadzu Shim-pack 150 L x 4.6 mm VP-ODS Column C18 on temperature 30 oC. The validation examination is based on specificity, precision, accuracy, limit of qualitative, quantitative limits, and linearity. Results of the research shows the average of area concentration 1 μg/ml, 2 μg/ml, and 5 μg/ml in consecutive are 34620.33, 79048.67, dan 181208.7 with retention time in 8.6-8.98 minute. Repeatability is clone 3 times and the RSD mean value obtained is � 2%. The detection limit at 0.1 μg/ml and limit of quantification at concententration 1 μg/ml. The equation of linear line y = 36046x+2182, with the value of R= 0.99. It can be concluded that the method used in the research posseses good validity. [Yogyakarta] : Universitas Gadjah Mada 2014 Thesis NonPeerReviewed , PRADITA RENDYAWAN and , drh. R. Gagak Donny Satria, M.P., M.Pd. (2014) VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT). UNSPECIFIED thesis, UNSPECIFIED. http://etd.ugm.ac.id/index.php?mod=penelitian_detail&sub=PenelitianDetail&act=view&typ=html&buku_id=71816 |
| spellingShingle | ETD , PRADITA RENDYAWAN , drh. R. Gagak Donny Satria, M.P., M.Pd. VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT) |
| title | VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT) |
| title_full | VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT) |
| title_fullStr | VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT) |
| title_full_unstemmed | VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT) |
| title_short | VALIDASI PROSEDUR ANALISIS DELTAMETHRIN PADA DAGING AYAM BROILER MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI (KCKT) |
| title_sort | validasi prosedur analisis deltamethrin pada daging ayam broiler menggunakan alat kromatografi cair kinerja tinggi kckt |
| topic | ETD |
| work_keys_str_mv | AT praditarendyawan validasiproseduranalisisdeltamethrinpadadagingayambroilermenggunakanalatkromatograficairkinerjatinggikckt AT drhrgagakdonnysatriampmpd validasiproseduranalisisdeltamethrinpadadagingayambroilermenggunakanalatkromatograficairkinerjatinggikckt |