2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid
In the title compound, C14H18N2O3, the carboxylic group is tilted by 12.00 (4)° with respect to the mean plane throught the benzimidazole ring system. The alcohol and carboxyl hydroxy groups are involved in intermolecular O-HO and O-HN hydrogen bonds, forming a two-dimensional network extending para...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2012
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| Subjects: | |
| Online Access: | http://irep.iium.edu.my/25383/1/sendreprint_rz2764_sh16.pdf |
| _version_ | 1825646747092779008 |
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| author | Hamzah, Nurasyikin Ngah, Nurziana Abd Hamid, Shafida Abdul Rahim, Aisyah Saad |
| author_facet | Hamzah, Nurasyikin Ngah, Nurziana Abd Hamid, Shafida Abdul Rahim, Aisyah Saad |
| author_sort | Hamzah, Nurasyikin |
| collection | IIUM |
| description | In the title compound, C14H18N2O3, the carboxylic group is tilted by 12.00 (4)° with respect to the mean plane throught the benzimidazole ring system. The alcohol and carboxyl hydroxy groups are involved in intermolecular O-HO and O-HN hydrogen bonds, forming a two-dimensional network extending parallel the ab plane. The network is further stabilized by weak C-HO interactions. The sec-butyl group is disordered over two sets of sites with refined occupancies of 0.484 (4) and 0.516 (4). |
| first_indexed | 2024-03-05T23:07:11Z |
| format | Article |
| id | oai:generic.eprints.org:25383 |
| institution | International Islamic University Malaysia |
| language | English |
| last_indexed | 2024-03-13T18:56:51Z |
| publishDate | 2012 |
| publisher | International Union of Crystallography |
| record_format | dspace |
| spelling | oai:generic.eprints.org:253832012-08-08T00:18:05Z http://irep.iium.edu.my/25383/ 2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid Hamzah, Nurasyikin Ngah, Nurziana Abd Hamid, Shafida Abdul Rahim, Aisyah Saad QD Chemistry In the title compound, C14H18N2O3, the carboxylic group is tilted by 12.00 (4)° with respect to the mean plane throught the benzimidazole ring system. The alcohol and carboxyl hydroxy groups are involved in intermolecular O-HO and O-HN hydrogen bonds, forming a two-dimensional network extending parallel the ab plane. The network is further stabilized by weak C-HO interactions. The sec-butyl group is disordered over two sets of sites with refined occupancies of 0.484 (4) and 0.516 (4). International Union of Crystallography 2012 Article PeerReviewed application/pdf en http://irep.iium.edu.my/25383/1/sendreprint_rz2764_sh16.pdf Hamzah, Nurasyikin and Ngah, Nurziana and Abd Hamid, Shafida and Abdul Rahim, Aisyah Saad (2012) 2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid. Acta Crystallographica Section E Structure Reports Online, E68 (7). o1995. ISSN 1600-5368 http://scripts.iucr.org/cgi-bin/paper?rz2764 10.1107/S1600536812023884 |
| spellingShingle | QD Chemistry Hamzah, Nurasyikin Ngah, Nurziana Abd Hamid, Shafida Abdul Rahim, Aisyah Saad 2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid |
| title | 2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid |
| title_full | 2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid |
| title_fullStr | 2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid |
| title_full_unstemmed | 2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid |
| title_short | 2-sec-Butyl-1-(2-hydroxyethyl)-1H-benzimidazole-5-carboxylic acid |
| title_sort | 2 sec butyl 1 2 hydroxyethyl 1h benzimidazole 5 carboxylic acid |
| topic | QD Chemistry |
| url | http://irep.iium.edu.my/25383/1/sendreprint_rz2764_sh16.pdf |
| work_keys_str_mv | AT hamzahnurasyikin 2secbutyl12hydroxyethyl1hbenzimidazole5carboxylicacid AT ngahnurziana 2secbutyl12hydroxyethyl1hbenzimidazole5carboxylicacid AT abdhamidshafida 2secbutyl12hydroxyethyl1hbenzimidazole5carboxylicacid AT abdulrahimaisyahsaad 2secbutyl12hydroxyethyl1hbenzimidazole5carboxylicacid |