Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication

Animal fats including lard (LD), beef fat (BF) and chicken fat (CF) are commonly used in food products. However, they raised some health and religious issues, therefore the simultaneous analysis of animal fats is necessary. The objective of this study was to employ FTIR spectroscopy in combination...

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Main Authors: Lestari, L.A., Rohman, Abdul, Prihandiwati, E., Aini, A.R., Irnawati, Irnawati, Khasanah, F.
Format: Article
Language:English
Published: Rynnye Lyan Resources 2022
Subjects:
Online Access:https://repository.ugm.ac.id/278661/1/Lestari_KKMK.pdf
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author Lestari, L.A.
Rohman, Abdul
Prihandiwati, E.
Aini, A.R.
Irnawati, Irnawati
Khasanah, F.
author_facet Lestari, L.A.
Rohman, Abdul
Prihandiwati, E.
Aini, A.R.
Irnawati, Irnawati
Khasanah, F.
author_sort Lestari, L.A.
collection UGM
description Animal fats including lard (LD), beef fat (BF) and chicken fat (CF) are commonly used in food products. However, they raised some health and religious issues, therefore the simultaneous analysis of animal fats is necessary. The objective of this study was to employ FTIR spectroscopy in combination with chemometrics of multivariate calibration for analysis of LD, CF, and BF in ternary systems simulta-neously. Animal fats were prepared using the rendering process of adipose tissues from corresponding animals. The obtained fats were used to prepare calibration and valida-tion samples. FTIR spectra scanned at the midinfrared region (4000-650 cm-1) were used as variables during calibration and validation modelling with the aid of multivariate calibrations. Based on optimization (wavenumbers region, FTIR spectral mode, and multivariate calibration types) using the parameter of the highest R2 values and lowest values of RMSEC and RMSEP, PLSR using a variable of normal FTIR spectral at the combined wavenumber regions of 3100-2750 and 1800-660 cm-1 for prediction of animal fats (LD, CF and BF) simultaneously. FTIR spectroscopy in combi-nation with multivariate calibrations could be a useful technique for analysis of animal fats in the ternary mixture, including analysis of lard for halal authentication.
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spelling oai:generic.eprints.org:2786612023-11-02T01:19:47Z https://repository.ugm.ac.id/278661/ Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication Lestari, L.A. Rohman, Abdul Prihandiwati, E. Aini, A.R. Irnawati, Irnawati Khasanah, F. Nutrition and Dietetics Animal fats including lard (LD), beef fat (BF) and chicken fat (CF) are commonly used in food products. However, they raised some health and religious issues, therefore the simultaneous analysis of animal fats is necessary. The objective of this study was to employ FTIR spectroscopy in combination with chemometrics of multivariate calibration for analysis of LD, CF, and BF in ternary systems simulta-neously. Animal fats were prepared using the rendering process of adipose tissues from corresponding animals. The obtained fats were used to prepare calibration and valida-tion samples. FTIR spectra scanned at the midinfrared region (4000-650 cm-1) were used as variables during calibration and validation modelling with the aid of multivariate calibrations. Based on optimization (wavenumbers region, FTIR spectral mode, and multivariate calibration types) using the parameter of the highest R2 values and lowest values of RMSEC and RMSEP, PLSR using a variable of normal FTIR spectral at the combined wavenumber regions of 3100-2750 and 1800-660 cm-1 for prediction of animal fats (LD, CF and BF) simultaneously. FTIR spectroscopy in combi-nation with multivariate calibrations could be a useful technique for analysis of animal fats in the ternary mixture, including analysis of lard for halal authentication. Rynnye Lyan Resources 2022-07-14 Article PeerReviewed application/pdf en https://repository.ugm.ac.id/278661/1/Lestari_KKMK.pdf Lestari, L.A. and Rohman, Abdul and Prihandiwati, E. and Aini, A.R. and Irnawati, Irnawati and Khasanah, F. (2022) Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication. Food Research, 6 (4). pp. 113-119. ISSN 2550-2166 https://www.myfoodresearch.com https://doi.org/10.26656/fr.2017.6(4).488
spellingShingle Nutrition and Dietetics
Lestari, L.A.
Rohman, Abdul
Prihandiwati, E.
Aini, A.R.
Irnawati, Irnawati
Khasanah, F.
Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication
title Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication
title_full Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication
title_fullStr Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication
title_full_unstemmed Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication
title_short Analysis of lard, chicken fat and beef fat in ternary mixture using FTIR spectroscopy and multivariate calibration for halal authentication
title_sort analysis of lard chicken fat and beef fat in ternary mixture using ftir spectroscopy and multivariate calibration for halal authentication
topic Nutrition and Dietetics
url https://repository.ugm.ac.id/278661/1/Lestari_KKMK.pdf
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