1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN
ABSTRACT The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in bo...
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| Format: | Article |
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[Yogyakarta] : Universitas Gadjah Mada
2008
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| _version_ | 1797019801420300288 |
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| author | AI-DOUH, Mohammed Hadi |
| author_facet | AI-DOUH, Mohammed Hadi |
| author_sort | AI-DOUH, Mohammed Hadi |
| collection | UGM |
| description | ABSTRACT
The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the
presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete
assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in both COCI3and
acetone-d6 are discussed, and the coupling constants J are reported in Hertz (Hz).
Keywords: 1HNMR |
| first_indexed | 2024-03-13T19:05:17Z |
| format | Article |
| id | oai:generic.eprints.org:27936 |
| institution | Universiti Gadjah Mada |
| last_indexed | 2024-03-13T19:05:17Z |
| publishDate | 2008 |
| publisher | [Yogyakarta] : Universitas Gadjah Mada |
| record_format | dspace |
| spelling | oai:generic.eprints.org:279362016-04-23T13:01:10Z https://repository.ugm.ac.id/27936/ 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN AI-DOUH, Mohammed Hadi Chemical Science Organic Chemistry Organic Chemical Synthesis ABSTRACT The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in both COCI3and acetone-d6 are discussed, and the coupling constants J are reported in Hertz (Hz). Keywords: 1HNMR [Yogyakarta] : Universitas Gadjah Mada 2008 Article PeerReviewed AI-DOUH, Mohammed Hadi (2008) 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN. Jurnal i-lib UGM, VIII (3). (Unpublished) http://i-lib.ugm.ac.id/jurnal/download.php?dataId=10999 |
| spellingShingle | Chemical Science Organic Chemistry Organic Chemical Synthesis AI-DOUH, Mohammed Hadi 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
| title | 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
| title_full | 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
| title_fullStr | 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
| title_full_unstemmed | 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
| title_short | 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
| title_sort | 1d and 2d nmr studies of benzyl o v anillin |
| topic | Chemical Science Organic Chemistry Organic Chemical Synthesis |
| work_keys_str_mv | AT aidouhmohammedhadi 1dand2dnmrstudiesofbenzylovanillin |