SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L)

ABSTRACT This research is aimed to primarily study the spectroscopy of ether fraction of from Jati wood (T. grandis, L). The stem bark of T.grandis, L was firstly extracted undergoes a ranux in methanol solvent. Further, the dried methanol crude extract was extracted with diethyl ether and moreover...

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Main Author: Perpustakaan UGM, i-lib
Format: Article
Published: [Yogyakarta] : Universitas Gadjah Mada 2009
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author Perpustakaan UGM, i-lib
author_facet Perpustakaan UGM, i-lib
author_sort Perpustakaan UGM, i-lib
collection UGM
description ABSTRACT This research is aimed to primarily study the spectroscopy of ether fraction of from Jati wood (T. grandis, L). The stem bark of T.grandis, L was firstly extracted undergoes a ranux in methanol solvent. Further, the dried methanol crude extract was extracted with diethyl ether and moreover separated its chemical constituents by using of column chromatography using degraded mixtures of n-hexane - ethyl acetate from 9:1 to 7:3. After a final column chromatography from the E fraction, a white needles crystal with a melting point of 295 - 297.5 °C was resulted. This results was then confirmed undergoes a spectroscopic analysis including UV, FTIR, H-NMR, and Mass spectroscopy to get an acid of 3{3-hydroxy-20(29)-lupen-28-oic or commonly known as betulinic acid. Keywords: betulinic acid, spectroscopy,primarily stud
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spelling oai:generic.eprints.org:280132014-06-18T00:24:39Z https://repository.ugm.ac.id/28013/ SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L) Perpustakaan UGM, i-lib Jurnal i-lib UGM ABSTRACT This research is aimed to primarily study the spectroscopy of ether fraction of from Jati wood (T. grandis, L). The stem bark of T.grandis, L was firstly extracted undergoes a ranux in methanol solvent. Further, the dried methanol crude extract was extracted with diethyl ether and moreover separated its chemical constituents by using of column chromatography using degraded mixtures of n-hexane - ethyl acetate from 9:1 to 7:3. After a final column chromatography from the E fraction, a white needles crystal with a melting point of 295 - 297.5 °C was resulted. This results was then confirmed undergoes a spectroscopic analysis including UV, FTIR, H-NMR, and Mass spectroscopy to get an acid of 3{3-hydroxy-20(29)-lupen-28-oic or commonly known as betulinic acid. Keywords: betulinic acid, spectroscopy,primarily stud [Yogyakarta] : Universitas Gadjah Mada 2009 Article NonPeerReviewed Perpustakaan UGM, i-lib (2009) SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L). Jurnal i-lib UGM. http://i-lib.ugm.ac.id/jurnal/download.php?dataId=11076
spellingShingle Jurnal i-lib UGM
Perpustakaan UGM, i-lib
SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L)
title SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L)
title_full SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L)
title_fullStr SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L)
title_full_unstemmed SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L)
title_short SPECTROSCOPICALSTUDYOF AN ETHER FRACTIONISOLATE FROM STEAM BARK OF" JATI" (Tectona grandls, L)
title_sort spectroscopicalstudyof an ether fractionisolate from steam bark of jati tectona grandls l
topic Jurnal i-lib UGM
work_keys_str_mv AT perpustakaanugmilib spectroscopicalstudyofanetherfractionisolatefromsteambarkofjatitectonagrandlsl