Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts

Synthesis of patchouli acetate and propionate from patchouli oil and carboxylic acids (acetic acid and propionic acid) has been carried out through an esterification reaction. The reaction was carried out at 100 °C for 3 h in the presence of homogeneous (HCl and H2SO4) and heterogeneous (activated z...

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Main Authors: Priatmoko, Priatmoko, Mardjan, Muhammad Idham Darussalam, Juniati, Vera
Format: Other
Published: Materials Science Forum 2022
Subjects:
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author Priatmoko, Priatmoko
Mardjan, Muhammad Idham Darussalam
Juniati, Vera
author_facet Priatmoko, Priatmoko
Mardjan, Muhammad Idham Darussalam
Juniati, Vera
author_sort Priatmoko, Priatmoko
collection UGM
description Synthesis of patchouli acetate and propionate from patchouli oil and carboxylic acids (acetic acid and propionic acid) has been carried out through an esterification reaction. The reaction was carried out at 100 °C for 3 h in the presence of homogeneous (HCl and H2SO4) and heterogeneous (activated zeolite) catalysts. The esterification products were characterized using Fourier Transform Infrared Spectrometer and Gas Chromatography-Mass Spectrometer. The results showed that the reaction using acetic acid as the acid precursor in the presence of HCl, H2SO4, and zeolite gave patchouli acetate in 42, 48, and 38%, respectively. In addition, the esterification of patchouli oil using propionic acid in the presence of HCl, H2SO4, and zeolite produced patchouli propionate in 40, 54, and 36%, respectively
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institution Universiti Gadjah Mada
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spelling oai:generic.eprints.org:2844832024-01-04T03:27:57Z https://repository.ugm.ac.id/284483/ Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts Priatmoko, Priatmoko Mardjan, Muhammad Idham Darussalam Juniati, Vera Chemical Science Synthesis of patchouli acetate and propionate from patchouli oil and carboxylic acids (acetic acid and propionic acid) has been carried out through an esterification reaction. The reaction was carried out at 100 °C for 3 h in the presence of homogeneous (HCl and H2SO4) and heterogeneous (activated zeolite) catalysts. The esterification products were characterized using Fourier Transform Infrared Spectrometer and Gas Chromatography-Mass Spectrometer. The results showed that the reaction using acetic acid as the acid precursor in the presence of HCl, H2SO4, and zeolite gave patchouli acetate in 42, 48, and 38%, respectively. In addition, the esterification of patchouli oil using propionic acid in the presence of HCl, H2SO4, and zeolite produced patchouli propionate in 40, 54, and 36%, respectively Materials Science Forum 2022 Other NonPeerReviewed Priatmoko, Priatmoko and Mardjan, Muhammad Idham Darussalam and Juniati, Vera (2022) Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts. Materials Science Forum. https://www.scientific.net/MSF.1061.157 10.4028/p-3cv57p
spellingShingle Chemical Science
Priatmoko, Priatmoko
Mardjan, Muhammad Idham Darussalam
Juniati, Vera
Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts
title Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts
title_full Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts
title_fullStr Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts
title_full_unstemmed Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts
title_short Synthesis of Patchouli Acetate and Propionate from Patchouli Oil Through Esterification Reaction Using Homogeneous and Heterogeneous Catalysts
title_sort synthesis of patchouli acetate and propionate from patchouli oil through esterification reaction using homogeneous and heterogeneous catalysts
topic Chemical Science
work_keys_str_mv AT priatmokopriatmoko synthesisofpatchouliacetateandpropionatefrompatchoulioilthroughesterificationreactionusinghomogeneousandheterogeneouscatalysts
AT mardjanmuhammadidhamdarussalam synthesisofpatchouliacetateandpropionatefrompatchoulioilthroughesterificationreactionusinghomogeneousandheterogeneouscatalysts
AT juniativera synthesisofpatchouliacetateandpropionatefrompatchoulioilthroughesterificationreactionusinghomogeneousandheterogeneouscatalysts