THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE
It was conducted a research about the addition effect of sulphanilic acid to the synthesis 3,4- methylenedioxybenzaldehyde from the isosafrole using reagents of sodium dichromate, sulphuric acid, and sulphanilic acid. The separation and purification of product were performed using the chromatograph...
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| Format: | Article |
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[Yogyakarta] : Universitas Gadjah Mada
2011
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| author | Perpustakaan UGM, i-lib |
| author_facet | Perpustakaan UGM, i-lib |
| author_sort | Perpustakaan UGM, i-lib |
| collection | UGM |
| description | It was conducted a research about the addition effect of sulphanilic acid to the synthesis 3,4- methylenedioxybenzaldehyde from the isosafrole using reagents of sodium dichromate, sulphuric acid, and sulphanilic acid. The separation and purification of product were performed using the chromatographycolumn. The
purity of the result was tested using thin layer chromatographyand determination of the melting point. Furthermore, it was identified its structure using infrared spectrophoto meter, 1H and 13C nuclear magnetic resonance spectrometry, and mass spectrometry. The experimental result showed that the percentage yield of 3,4- methylenedioxybenzaldehyde with addition sulphanilic acid was 79.54%. |
| first_indexed | 2024-03-13T19:10:01Z |
| format | Article |
| id | oai:generic.eprints.org:29248 |
| institution | Universiti Gadjah Mada |
| last_indexed | 2024-03-13T19:10:01Z |
| publishDate | 2011 |
| publisher | [Yogyakarta] : Universitas Gadjah Mada |
| record_format | dspace |
| spelling | oai:generic.eprints.org:292482014-06-18T00:23:21Z https://repository.ugm.ac.id/29248/ THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE Perpustakaan UGM, i-lib Jurnal i-lib UGM It was conducted a research about the addition effect of sulphanilic acid to the synthesis 3,4- methylenedioxybenzaldehyde from the isosafrole using reagents of sodium dichromate, sulphuric acid, and sulphanilic acid. The separation and purification of product were performed using the chromatographycolumn. The purity of the result was tested using thin layer chromatographyand determination of the melting point. Furthermore, it was identified its structure using infrared spectrophoto meter, 1H and 13C nuclear magnetic resonance spectrometry, and mass spectrometry. The experimental result showed that the percentage yield of 3,4- methylenedioxybenzaldehyde with addition sulphanilic acid was 79.54%. [Yogyakarta] : Universitas Gadjah Mada 2011 Article NonPeerReviewed Perpustakaan UGM, i-lib (2011) THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE. Jurnal i-lib UGM. http://i-lib.ugm.ac.id/jurnal/download.php?dataId=12311 |
| spellingShingle | Jurnal i-lib UGM Perpustakaan UGM, i-lib THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE |
| title | THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE |
| title_full | THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE |
| title_fullStr | THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE |
| title_full_unstemmed | THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE |
| title_short | THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE |
| title_sort | addition effect of sulphanilic acid to the synthesis of 3 4 methylenedioxybenzaldehyde |
| topic | Jurnal i-lib UGM |
| work_keys_str_mv | AT perpustakaanugmilib theadditioneffectofsulphanilicacidtothesynthesisof34methylenedioxybenzaldehyde AT perpustakaanugmilib additioneffectofsulphanilicacidtothesynthesisof34methylenedioxybenzaldehyde |