VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES
<p>Validation of voltammetric method for, Cd, Pb, Zn, Ni, Co, Al and Fe determination in biological samples, has<br /> been done using standard reference materials. Anodic stripping voltammetry has been used on Cu, Cd, Pb and Zn<br /> determination. Mean while adsorptive cathodic s...
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| Format: | Article |
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[Yogyakarta] : Fak. MIPA Universitas Gadjah Mada
2007
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| _version_ | 1797031369655713792 |
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| author | , Saryati, Sutisna, and Rukihati |
| author_facet | , Saryati, Sutisna, and Rukihati |
| author_sort | , Saryati, Sutisna, and Rukihati |
| collection | UGM |
| description | <p>Validation of voltammetric method for, Cd, Pb, Zn, Ni, Co, Al and Fe determination in biological samples, has<br />
been done using standard reference materials. Anodic stripping voltammetry has been used on Cu, Cd, Pb and Zn<br />
determination. Mean while adsorptive cathodic stripping voltammetry, in dimethylglioxime complexing agent has<br />
been used for Ni and Co determination, and finally adsorptive cathodic stripping voltammetry in solochrome violete<br />
complexing agent used on Al and Fe determination. The validation method consist of a linearity of standard<br />
calibration, trueness and precision. The validation carried out by using standard reference materials of NIST SRM<br />
1566 b Oyster Tissue and CRM NIES No. 9 Sargasso. Sample digestion has been done by using the micro wave<br />
digester apparatus. It has been shown that the standard curves linearity for all ions were good enough. The ions<br />
determinations in a material standard have a recovery of about 92.2 -104.3 %. From the &ldquo |
| first_indexed | 2024-03-13T22:20:40Z |
| format | Article |
| id | oai:generic.eprints.org:93899 |
| institution | Universiti Gadjah Mada |
| last_indexed | 2024-03-13T22:20:40Z |
| publishDate | 2007 |
| publisher | [Yogyakarta] : Fak. MIPA Universitas Gadjah Mada |
| record_format | dspace |
| spelling | oai:generic.eprints.org:938992014-11-28T07:36:21Z https://repository.ugm.ac.id/93899/ VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES , Saryati, Sutisna, and Rukihati <p>Validation of voltammetric method for, Cd, Pb, Zn, Ni, Co, Al and Fe determination in biological samples, has<br /> been done using standard reference materials. Anodic stripping voltammetry has been used on Cu, Cd, Pb and Zn<br /> determination. Mean while adsorptive cathodic stripping voltammetry, in dimethylglioxime complexing agent has<br /> been used for Ni and Co determination, and finally adsorptive cathodic stripping voltammetry in solochrome violete<br /> complexing agent used on Al and Fe determination. The validation method consist of a linearity of standard<br /> calibration, trueness and precision. The validation carried out by using standard reference materials of NIST SRM<br /> 1566 b Oyster Tissue and CRM NIES No. 9 Sargasso. Sample digestion has been done by using the micro wave<br /> digester apparatus. It has been shown that the standard curves linearity for all ions were good enough. The ions<br /> determinations in a material standard have a recovery of about 92.2 -104.3 %. From the &ldquo [Yogyakarta] : Fak. MIPA Universitas Gadjah Mada 2007 Article NonPeerReviewed , Saryati, Sutisna, and Rukihati (2007) VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES. text. http://repository.ugm.ac.id/digitasi/index.php?module=cari_hasil_full&idbuku=1694 |
| spellingShingle | , Saryati, Sutisna, and Rukihati VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES |
| title | VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES |
| title_full | VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES |
| title_fullStr | VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES |
| title_full_unstemmed | VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES |
| title_short | VALIDATION OF VOLTAMMETRY METHOD FOR TRACE METALS ANALYSIS IN BIOLOGICAL SAMPLES |
| title_sort | validation of voltammetry method for trace metals analysis in biological samples |
| work_keys_str_mv | AT saryatisutisnaandrukihati validationofvoltammetrymethodfortracemetalsanalysisinbiologicalsamples |