SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN

<p>Cationic water-soluble chitosan was synthesized by conjugating 3-chloro-hydroxy-propyltrimethylammonium chloride onto chitosan chain. Varying the molar ratio of 3-chloro-hydroxy-propyltrimethylammonium chloride to chitosan from 3:1 to 6:1 produced chitosan with variation of substitution deg...

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Main Author: , Agus Haryono, and Dewi Sondari
Format: Article
Published: [Yogyakarta] : Fak. MIPA Universitas Gadjah Mada 2007
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author , Agus Haryono, and Dewi Sondari
author_facet , Agus Haryono, and Dewi Sondari
author_sort , Agus Haryono, and Dewi Sondari
collection UGM
description <p>Cationic water-soluble chitosan was synthesized by conjugating 3-chloro-hydroxy-propyltrimethylammonium chloride onto chitosan chain. Varying the molar ratio of 3-chloro-hydroxy-propyltrimethylammonium chloride to chitosan from 3:1 to 6:1 produced chitosan with variation of substitution degree. The molecular weight of chitosan was determined by intrinsic viscosity measurements in 0.25 M acetic acid / 0.25 M sodium acetate at 25oC. FTIR measurements were performed to analyze the chemical composition of the cationic water-soluble chitosan. 1H NMR spectra were obtained to confirm the successful conjugation onto chitosan chain. Water solubility of obtained cationic polymers was measured using UV-vis spectrophotometer at 600 nm.</p>
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spelling oai:generic.eprints.org:939512014-11-28T07:36:09Z https://repository.ugm.ac.id/93951/ SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN , Agus Haryono, and Dewi Sondari <p>Cationic water-soluble chitosan was synthesized by conjugating 3-chloro-hydroxy-propyltrimethylammonium chloride onto chitosan chain. Varying the molar ratio of 3-chloro-hydroxy-propyltrimethylammonium chloride to chitosan from 3:1 to 6:1 produced chitosan with variation of substitution degree. The molecular weight of chitosan was determined by intrinsic viscosity measurements in 0.25 M acetic acid / 0.25 M sodium acetate at 25oC. FTIR measurements were performed to analyze the chemical composition of the cationic water-soluble chitosan. 1H NMR spectra were obtained to confirm the successful conjugation onto chitosan chain. Water solubility of obtained cationic polymers was measured using UV-vis spectrophotometer at 600 nm.</p> [Yogyakarta] : Fak. MIPA Universitas Gadjah Mada 2007 Article NonPeerReviewed , Agus Haryono, and Dewi Sondari (2007) SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN. text. http://repository.ugm.ac.id/digitasi/index.php?module=cari_hasil_full&idbuku=1750
spellingShingle , Agus Haryono, and Dewi Sondari
SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN
title SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN
title_full SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN
title_fullStr SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN
title_full_unstemmed SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN
title_short SYNTHESIS OF CATIONIC WATER SOLUBLE CHITOSAN HAVING QUARTERNARY AMMONIUM GROUP SIDE CHAIN
title_sort synthesis of cationic water soluble chitosan having quarternary ammonium group side chain
work_keys_str_mv AT agusharyonoanddewisondari synthesisofcationicwatersolublechitosanhavingquarternaryammoniumgroupsidechain