Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran
2,6-pyridinedihydroxamic acid (2,6-pyha) was synthesized and characterized their complexation properties with iron(III) metal. The percentages compositions of each elements in 2,6-pyha and iron(III) complex was determined by elemental analysis. It shows that the percentages C,H and N in 2,6-pyha are...
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| Format: | Student Project |
| Language: | English |
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Faculty of Applied Sciences
2009
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| Online Access: | https://ir.uitm.edu.my/id/eprint/1034/1/PPb_SUHANA%20MISRAN%20AS%2009_5%20P01.pdf |
| _version_ | 1796899267510534144 |
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| author | Misran, Suhana |
| author_facet | Misran, Suhana |
| author_sort | Misran, Suhana |
| collection | UITM |
| description | 2,6-pyridinedihydroxamic acid (2,6-pyha) was synthesized and characterized their complexation properties with iron(III) metal. The percentages compositions of each elements in 2,6-pyha and iron(III) complex was determined by elemental analysis. It shows that the percentages C,H and N in 2,6-pyha are 44.48%, 3.63% and 21.12%. While in iron(III) complex, the percentages compositions are 32.72%, 3.60% and 18.74% which corresponds to C, H and N. It is indicated in the IR spectra of 2,6-pyha that the vо ̵ н, vN ̵ н and vc ̵ o are at 2822.75 cm⁻¹, 3153.31 cm⁻¹ and 1669.48 cm⁻¹ respectively. While the IR spectra for iron(III) complex shows the shifting value at N-H bond which then was confirmed there is a coordination mode between nitrogen from pyridine ring with iron(III) metal. The ¹H NMR spectra shows for 2,6-pyha, the presence of O-H resonance at 11.85 ppm, N-H resonance at 9.331 ppm and H resonance from disubstituted pyridine ring at 8.137 ppm. |
| first_indexed | 2024-03-06T01:18:32Z |
| format | Student Project |
| id | oai:ir.uitm.edu.my:1034 |
| institution | Universiti Teknologi MARA |
| language | English |
| last_indexed | 2024-03-06T01:18:32Z |
| publishDate | 2009 |
| publisher | Faculty of Applied Sciences |
| record_format | dspace |
| spelling | oai:ir.uitm.edu.my:10342018-10-22T03:42:23Z https://ir.uitm.edu.my/id/eprint/1034/ Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran Misran, Suhana QD Chemistry 2,6-pyridinedihydroxamic acid (2,6-pyha) was synthesized and characterized their complexation properties with iron(III) metal. The percentages compositions of each elements in 2,6-pyha and iron(III) complex was determined by elemental analysis. It shows that the percentages C,H and N in 2,6-pyha are 44.48%, 3.63% and 21.12%. While in iron(III) complex, the percentages compositions are 32.72%, 3.60% and 18.74% which corresponds to C, H and N. It is indicated in the IR spectra of 2,6-pyha that the vо ̵ н, vN ̵ н and vc ̵ o are at 2822.75 cm⁻¹, 3153.31 cm⁻¹ and 1669.48 cm⁻¹ respectively. While the IR spectra for iron(III) complex shows the shifting value at N-H bond which then was confirmed there is a coordination mode between nitrogen from pyridine ring with iron(III) metal. The ¹H NMR spectra shows for 2,6-pyha, the presence of O-H resonance at 11.85 ppm, N-H resonance at 9.331 ppm and H resonance from disubstituted pyridine ring at 8.137 ppm. Faculty of Applied Sciences 2009 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/1034/1/PPb_SUHANA%20MISRAN%20AS%2009_5%20P01.pdf Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran. (2009) [Student Project] <http://terminalib.uitm.edu.my/1034.pdf> (Unpublished) |
| spellingShingle | QD Chemistry Misran, Suhana Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran |
| title | Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran |
| title_full | Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran |
| title_fullStr | Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran |
| title_full_unstemmed | Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran |
| title_short | Synthesis and characterization of 2,6-pyridinedihydroxamic acid and its iron(III) complex / Suhana Misran |
| title_sort | synthesis and characterization of 2 6 pyridinedihydroxamic acid and its iron iii complex suhana misran |
| topic | QD Chemistry |
| url | https://ir.uitm.edu.my/id/eprint/1034/1/PPb_SUHANA%20MISRAN%20AS%2009_5%20P01.pdf |
| work_keys_str_mv | AT misransuhana synthesisandcharacterizationof26pyridinedihydroxamicacidanditsironiiicomplexsuhanamisran |