Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim
Solid Phase Microextraction (SPME) method of identifying accelerants from fire debris is developed. Experimental design methodology was used to evaluate the simultaneous effect of SPME operating variables (extraction time, extraction temperature, desorption time) on the extraction of target analytes...
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Format: | Article |
Language: | English |
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Faculty of Applied Sciences
2005
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Online Access: | https://ir.uitm.edu.my/id/eprint/11789/1/AJ_ABDUL%20AZIZ%20HARON%20SL%2005.pdf |
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author | Haron, Abdul Aziz Saim, Nor'ashikin |
author_facet | Haron, Abdul Aziz Saim, Nor'ashikin |
author_sort | Haron, Abdul Aziz |
collection | UITM |
description | Solid Phase Microextraction (SPME) method of identifying accelerants from fire debris is developed. Experimental design methodology was used to evaluate the simultaneous effect of SPME operating variables (extraction time, extraction temperature, desorption time) on the extraction of target analytes (benzene, toluene, xylene and hexadecane). The results showed that extraction temperature
and extraction time were the more significant factors. Optimum operating conditions for SPME were determined using a response surface method. The results indicate that SPME is capable of analyzing accelerants from fire debris. |
first_indexed | 2024-03-06T01:24:51Z |
format | Article |
id | oai:ir.uitm.edu.my:11789 |
institution | Universiti Teknologi MARA |
language | English |
last_indexed | 2024-03-06T01:24:51Z |
publishDate | 2005 |
publisher | Faculty of Applied Sciences |
record_format | dspace |
spelling | oai:ir.uitm.edu.my:117892016-09-06T04:53:53Z https://ir.uitm.edu.my/id/eprint/11789/ Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim scilett Haron, Abdul Aziz Saim, Nor'ashikin QD Chemistry Solid Phase Microextraction (SPME) method of identifying accelerants from fire debris is developed. Experimental design methodology was used to evaluate the simultaneous effect of SPME operating variables (extraction time, extraction temperature, desorption time) on the extraction of target analytes (benzene, toluene, xylene and hexadecane). The results showed that extraction temperature and extraction time were the more significant factors. Optimum operating conditions for SPME were determined using a response surface method. The results indicate that SPME is capable of analyzing accelerants from fire debris. Faculty of Applied Sciences 2005 Article PeerReviewed text en https://ir.uitm.edu.my/id/eprint/11789/1/AJ_ABDUL%20AZIZ%20HARON%20SL%2005.pdf Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim. (2005) Science Letters <https://ir.uitm.edu.my/view/publication/Science_Letters/>, 2 (1). pp. 55-61. ISSN 1675-7785 |
spellingShingle | QD Chemistry Haron, Abdul Aziz Saim, Nor'ashikin Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim |
title | Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim |
title_full | Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim |
title_fullStr | Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim |
title_full_unstemmed | Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim |
title_short | Developing a solid phase microextraction method for the identification of accelerants in fire debris / Abdul Aziz Haron and Nor'ashikin Saim |
title_sort | developing a solid phase microextraction method for the identification of accelerants in fire debris abdul aziz haron and nor ashikin saim |
topic | QD Chemistry |
url | https://ir.uitm.edu.my/id/eprint/11789/1/AJ_ABDUL%20AZIZ%20HARON%20SL%2005.pdf |
work_keys_str_mv | AT haronabdulaziz developingasolidphasemicroextractionmethodfortheidentificationofaccelerantsinfiredebrisabdulazizharonandnorashikinsaim AT saimnorashikin developingasolidphasemicroextractionmethodfortheidentificationofaccelerantsinfiredebrisabdulazizharonandnorashikinsaim |