2-C-Methyl-D-allono-1,4-lactone
The relative stereochemistry of the compound 2-c-methyl-D-allono-1,4-lactone was established using X ray crystallographic analysis. The absolute stereochemistry was defined by the use of D-ribonolactone as a starting material. All H atoms were observed in a difference electron density map and were r...
Huvudupphovsmän: | , , , , |
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Materialtyp: | Journal article |
Språk: | English |
Publicerad: |
2005
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_version_ | 1826262784109707264 |
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author | Harding, C Watkin, D Sawyer, N Jenkinson, S Fleet, G |
author_facet | Harding, C Watkin, D Sawyer, N Jenkinson, S Fleet, G |
author_sort | Harding, C |
collection | OXFORD |
description | The relative stereochemistry of the compound 2-c-methyl-D-allono-1,4-lactone was established using X ray crystallographic analysis. The absolute stereochemistry was defined by the use of D-ribonolactone as a starting material. All H atoms were observed in a difference electron density map and were refined using slack restraints to optimize their geometry. The crystal structure was made up of layers of strongly hydrogen-bonded molecules, which were found to be lying in the ab plane. |
first_indexed | 2024-03-06T19:41:33Z |
format | Journal article |
id | oxford-uuid:20d89f30-2103-4c59-ad18-bca5cdf281e8 |
institution | University of Oxford |
language | English |
last_indexed | 2024-03-06T19:41:33Z |
publishDate | 2005 |
record_format | dspace |
spelling | oxford-uuid:20d89f30-2103-4c59-ad18-bca5cdf281e82022-03-26T11:29:53Z2-C-Methyl-D-allono-1,4-lactoneJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:20d89f30-2103-4c59-ad18-bca5cdf281e8EnglishSymplectic Elements at Oxford2005Harding, CWatkin, DSawyer, NJenkinson, SFleet, GThe relative stereochemistry of the compound 2-c-methyl-D-allono-1,4-lactone was established using X ray crystallographic analysis. The absolute stereochemistry was defined by the use of D-ribonolactone as a starting material. All H atoms were observed in a difference electron density map and were refined using slack restraints to optimize their geometry. The crystal structure was made up of layers of strongly hydrogen-bonded molecules, which were found to be lying in the ab plane. |
spellingShingle | Harding, C Watkin, D Sawyer, N Jenkinson, S Fleet, G 2-C-Methyl-D-allono-1,4-lactone |
title | 2-C-Methyl-D-allono-1,4-lactone |
title_full | 2-C-Methyl-D-allono-1,4-lactone |
title_fullStr | 2-C-Methyl-D-allono-1,4-lactone |
title_full_unstemmed | 2-C-Methyl-D-allono-1,4-lactone |
title_short | 2-C-Methyl-D-allono-1,4-lactone |
title_sort | 2 c methyl d allono 1 4 lactone |
work_keys_str_mv | AT hardingc 2cmethyldallono14lactone AT watkind 2cmethyldallono14lactone AT sawyern 2cmethyldallono14lactone AT jenkinsons 2cmethyldallono14lactone AT fleetg 2cmethyldallono14lactone |