Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material

ODS steels are promising materials for Sodium cooled Fast Reactors since their fine distribution of nano-clusters confers excellent mechanical properties. However, the nano-feature stability needs to be assessed under neutron irradiation. Before irradiation, the characterizations show that nano-part...

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Main Authors: Ribis, J, Lozano-Perez, S
Format: Journal article
Language:English
Published: 2014
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author Ribis, J
Lozano-Perez, S
author_facet Ribis, J
Lozano-Perez, S
author_sort Ribis, J
collection OXFORD
description ODS steels are promising materials for Sodium cooled Fast Reactors since their fine distribution of nano-clusters confers excellent mechanical properties. However, the nano-feature stability needs to be assessed under neutron irradiation. Before irradiation, the characterizations show that nano-particles are finely distributed within the ferritic matrix and are identified to have a pyrochlore type structure. After irradiation of the MA957 alloy in the Phenix French reactor at 412 C up to 50 dpa and 430 C up to 75 dpa, transmission electron microscopy characterization reveals a very slight density fall but no distinguishable difference in nano-features size before and after irradiation. In addition, after both irradiations, the nano-oxides are still (Y, Ti, O) compounds with orientation relationship with the matrix. A multislice simulation of high resolution images suggests that nano-particles still have a fcc pyrochlore type structure after irradiation. A possible change of lattice parameter seems to be highlighted, possibly due to disordering by cascade effect. © 2013 Elsevier B.V. All rights reserved.
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spelling oxford-uuid:2b9d0efc-d344-4107-9420-60507d5e83572022-03-26T12:31:54ZNano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened materialJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:2b9d0efc-d344-4107-9420-60507d5e8357EnglishSymplectic Elements at Oxford2014Ribis, JLozano-Perez, SODS steels are promising materials for Sodium cooled Fast Reactors since their fine distribution of nano-clusters confers excellent mechanical properties. However, the nano-feature stability needs to be assessed under neutron irradiation. Before irradiation, the characterizations show that nano-particles are finely distributed within the ferritic matrix and are identified to have a pyrochlore type structure. After irradiation of the MA957 alloy in the Phenix French reactor at 412 C up to 50 dpa and 430 C up to 75 dpa, transmission electron microscopy characterization reveals a very slight density fall but no distinguishable difference in nano-features size before and after irradiation. In addition, after both irradiations, the nano-oxides are still (Y, Ti, O) compounds with orientation relationship with the matrix. A multislice simulation of high resolution images suggests that nano-particles still have a fcc pyrochlore type structure after irradiation. A possible change of lattice parameter seems to be highlighted, possibly due to disordering by cascade effect. © 2013 Elsevier B.V. All rights reserved.
spellingShingle Ribis, J
Lozano-Perez, S
Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material
title Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material
title_full Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material
title_fullStr Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material
title_full_unstemmed Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material
title_short Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material
title_sort nano cluster stability following neutron irradiation in ma957 oxide dispersion strengthened material
work_keys_str_mv AT ribisj nanoclusterstabilityfollowingneutronirradiationinma957oxidedispersionstrengthenedmaterial
AT lozanoperezs nanoclusterstabilityfollowingneutronirradiationinma957oxidedispersionstrengthenedmaterial