PROCESSING AND PROPERTIES OF AL2O3/SIC NANOCOMPOSITES

Alumina/SiC nanocomposites were produced by mechanical mixture of commercial powders. The preparation steps involved the vigorous mixing of the powders and drying under conditions where the homogeneous mixture was kept stable, Pressureless sintering of die-pressed powders achieved reasonable densiti...

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Main Authors: Borsa, C, Jiao, S, Todd, R, Brook, R
Format: Journal article
Language:English
Published: 1995
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author Borsa, C
Jiao, S
Todd, R
Brook, R
author_facet Borsa, C
Jiao, S
Todd, R
Brook, R
author_sort Borsa, C
collection OXFORD
description Alumina/SiC nanocomposites were produced by mechanical mixture of commercial powders. The preparation steps involved the vigorous mixing of the powders and drying under conditions where the homogeneous mixture was kept stable, Pressureless sintering of die-pressed powders achieved reasonable densities (similar to 97% theoretical density) for 2.5wt% of SiC on sintering at 2073K. Higher SIC contents strongly reduced the sintered density. The use of a more reactive alumina (finer matrix powder) gave similar results, Hot pressing at 1973 K/1 h/25 MPa produced high-density materials for SiC contents Bs high as 20 wt%. Transmission and scanning electron microscopy analysis showed that the SiC particles were well distributed and were situated both inside the grains and on the grain boundaries of the alumina matrix, The SiC strongly inhibited grain growth in the matrix in keeping with the Zener model. The bend strength increased as the SiC content increased, a result partly explained by the grain size refinement. The strength improvement of 20% over monolithic was explained In terms of the change to an intergranular fracture mode.
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spelling oxford-uuid:319e1c2a-873c-46fb-8443-bbabe0b8ddf32022-03-26T13:09:00ZPROCESSING AND PROPERTIES OF AL2O3/SIC NANOCOMPOSITESJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:319e1c2a-873c-46fb-8443-bbabe0b8ddf3EnglishSymplectic Elements at Oxford1995Borsa, CJiao, STodd, RBrook, RAlumina/SiC nanocomposites were produced by mechanical mixture of commercial powders. The preparation steps involved the vigorous mixing of the powders and drying under conditions where the homogeneous mixture was kept stable, Pressureless sintering of die-pressed powders achieved reasonable densities (similar to 97% theoretical density) for 2.5wt% of SiC on sintering at 2073K. Higher SIC contents strongly reduced the sintered density. The use of a more reactive alumina (finer matrix powder) gave similar results, Hot pressing at 1973 K/1 h/25 MPa produced high-density materials for SiC contents Bs high as 20 wt%. Transmission and scanning electron microscopy analysis showed that the SiC particles were well distributed and were situated both inside the grains and on the grain boundaries of the alumina matrix, The SiC strongly inhibited grain growth in the matrix in keeping with the Zener model. The bend strength increased as the SiC content increased, a result partly explained by the grain size refinement. The strength improvement of 20% over monolithic was explained In terms of the change to an intergranular fracture mode.
spellingShingle Borsa, C
Jiao, S
Todd, R
Brook, R
PROCESSING AND PROPERTIES OF AL2O3/SIC NANOCOMPOSITES
title PROCESSING AND PROPERTIES OF AL2O3/SIC NANOCOMPOSITES
title_full PROCESSING AND PROPERTIES OF AL2O3/SIC NANOCOMPOSITES
title_fullStr PROCESSING AND PROPERTIES OF AL2O3/SIC NANOCOMPOSITES
title_full_unstemmed PROCESSING AND PROPERTIES OF AL2O3/SIC NANOCOMPOSITES
title_short PROCESSING AND PROPERTIES OF AL2O3/SIC NANOCOMPOSITES
title_sort processing and properties of al2o3 sic nanocomposites
work_keys_str_mv AT borsac processingandpropertiesofal2o3sicnanocomposites
AT jiaos processingandpropertiesofal2o3sicnanocomposites
AT toddr processingandpropertiesofal2o3sicnanocomposites
AT brookr processingandpropertiesofal2o3sicnanocomposites