Microstructural characterization of Y2O3 ODS-Fe-Cr model alloys

Two Fe-12 wt% Cr alloys, one containing 0.4 wt% Y2O3 and the other Y2O3-free, have been produced by mechanical alloying followed by hot isostatic pressing. These oxide dispersion strengthened and reference alloys were characterized both in the as-HIPed state and after tempering by transmission elect...

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Main Authors: de Castro, V, Leguey, T, Munoz, A, Monge, M, Pareja, R, Marquis, E, Lozano-Perez, S, Jenkins, M
Formato: Conference item
Publicado em: 2009
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author de Castro, V
Leguey, T
Munoz, A
Monge, M
Pareja, R
Marquis, E
Lozano-Perez, S
Jenkins, M
author_facet de Castro, V
Leguey, T
Munoz, A
Monge, M
Pareja, R
Marquis, E
Lozano-Perez, S
Jenkins, M
author_sort de Castro, V
collection OXFORD
description Two Fe-12 wt% Cr alloys, one containing 0.4 wt% Y2O3 and the other Y2O3-free, have been produced by mechanical alloying followed by hot isostatic pressing. These oxide dispersion strengthened and reference alloys were characterized both in the as-HIPed state and after tempering by transmission electron microscopy and atom-probe tomography. The as-HIPed alloys exhibited the characteristic microstructure of lath martensite and contained a high density of dislocations. Small voids with sizes <10 nm were also observed. Both alloys also contained M3C and M23C6 carbides (M = Cr, Fe) probably as a result of C ingress during milling. After tempering at 1023 K for 4 h the microstructures had partially recovered. In the recovered regions, martensite laths were replaced by equiaxed grains in which M23C6 carbides decorated the grain boundaries. In the ODS alloy nanoparticles containing Y were commonly observed within grains, although they were also present at grain boundaries and adjacent to large carbides. © 2009 Elsevier B.V. All rights reserved.
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spelling oxford-uuid:4193f3a7-bbdc-4642-a04f-51946cb3fb5f2022-03-26T14:44:30ZMicrostructural characterization of Y2O3 ODS-Fe-Cr model alloysConference itemhttp://purl.org/coar/resource_type/c_5794uuid:4193f3a7-bbdc-4642-a04f-51946cb3fb5fSymplectic Elements at Oxford2009de Castro, VLeguey, TMunoz, AMonge, MPareja, RMarquis, ELozano-Perez, SJenkins, MTwo Fe-12 wt% Cr alloys, one containing 0.4 wt% Y2O3 and the other Y2O3-free, have been produced by mechanical alloying followed by hot isostatic pressing. These oxide dispersion strengthened and reference alloys were characterized both in the as-HIPed state and after tempering by transmission electron microscopy and atom-probe tomography. The as-HIPed alloys exhibited the characteristic microstructure of lath martensite and contained a high density of dislocations. Small voids with sizes <10 nm were also observed. Both alloys also contained M3C and M23C6 carbides (M = Cr, Fe) probably as a result of C ingress during milling. After tempering at 1023 K for 4 h the microstructures had partially recovered. In the recovered regions, martensite laths were replaced by equiaxed grains in which M23C6 carbides decorated the grain boundaries. In the ODS alloy nanoparticles containing Y were commonly observed within grains, although they were also present at grain boundaries and adjacent to large carbides. © 2009 Elsevier B.V. All rights reserved.
spellingShingle de Castro, V
Leguey, T
Munoz, A
Monge, M
Pareja, R
Marquis, E
Lozano-Perez, S
Jenkins, M
Microstructural characterization of Y2O3 ODS-Fe-Cr model alloys
title Microstructural characterization of Y2O3 ODS-Fe-Cr model alloys
title_full Microstructural characterization of Y2O3 ODS-Fe-Cr model alloys
title_fullStr Microstructural characterization of Y2O3 ODS-Fe-Cr model alloys
title_full_unstemmed Microstructural characterization of Y2O3 ODS-Fe-Cr model alloys
title_short Microstructural characterization of Y2O3 ODS-Fe-Cr model alloys
title_sort microstructural characterization of y2o3 ods fe cr model alloys
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