Evolution of thermal and mechanical properties of Nitinol wire as a function of ageing treatment conditions

As-received and cold-worked 55Ni–45Ti wt% Nitinol wire samples were subjected to various ageing treatments. Experiments show that the properties of as-received Nitinol, including microstructure, critical temperatures in thermally induced phase transformation, and critical stresses/strains in mechani...

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Main Authors: Wang, Z, Everaerts, J, Salvati, E, Korsunsky, A
Format: Journal article
Language:English
Published: Elsevier 2019
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author Wang, Z
Everaerts, J
Salvati, E
Korsunsky, A
author_facet Wang, Z
Everaerts, J
Salvati, E
Korsunsky, A
author_sort Wang, Z
collection OXFORD
description As-received and cold-worked 55Ni–45Ti wt% Nitinol wire samples were subjected to various ageing treatments. Experiments show that the properties of as-received Nitinol, including microstructure, critical temperatures in thermally induced phase transformation, and critical stresses/strains in mechanically induced phase transformation, change significantly after ageing process at 773 K for different durations ranging from 10 min to 5 h. BSE and EBSD/EDS analysis shows that the predominant microstructural evolution is a large increase in Ni4Ti3 precipitate volume fraction, while grain growth is negligible. DSC results show that as-received material exhibits little to no phase transformation during heating-cooling cycling at 5K/min, while various ageing durations lead to the emergence of phase transformation that occurs at different critical temperatures. Tensile loading experiments conducted using a test rig equipped with a heater revealed the evolution of mechanically induced phase transformation behaviour. Mathematical models are proposed to predict the dependence of critical temperatures and critical stresses/strains on the ageing treatment conditions and alloy composition.
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spelling oxford-uuid:45b710c5-cbb2-4c37-b43c-4fc596558e722022-03-26T15:09:28ZEvolution of thermal and mechanical properties of Nitinol wire as a function of ageing treatment conditionsJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:45b710c5-cbb2-4c37-b43c-4fc596558e72EnglishSymplectic Elements at OxfordElsevier2019Wang, ZEveraerts, JSalvati, EKorsunsky, AAs-received and cold-worked 55Ni–45Ti wt% Nitinol wire samples were subjected to various ageing treatments. Experiments show that the properties of as-received Nitinol, including microstructure, critical temperatures in thermally induced phase transformation, and critical stresses/strains in mechanically induced phase transformation, change significantly after ageing process at 773 K for different durations ranging from 10 min to 5 h. BSE and EBSD/EDS analysis shows that the predominant microstructural evolution is a large increase in Ni4Ti3 precipitate volume fraction, while grain growth is negligible. DSC results show that as-received material exhibits little to no phase transformation during heating-cooling cycling at 5K/min, while various ageing durations lead to the emergence of phase transformation that occurs at different critical temperatures. Tensile loading experiments conducted using a test rig equipped with a heater revealed the evolution of mechanically induced phase transformation behaviour. Mathematical models are proposed to predict the dependence of critical temperatures and critical stresses/strains on the ageing treatment conditions and alloy composition.
spellingShingle Wang, Z
Everaerts, J
Salvati, E
Korsunsky, A
Evolution of thermal and mechanical properties of Nitinol wire as a function of ageing treatment conditions
title Evolution of thermal and mechanical properties of Nitinol wire as a function of ageing treatment conditions
title_full Evolution of thermal and mechanical properties of Nitinol wire as a function of ageing treatment conditions
title_fullStr Evolution of thermal and mechanical properties of Nitinol wire as a function of ageing treatment conditions
title_full_unstemmed Evolution of thermal and mechanical properties of Nitinol wire as a function of ageing treatment conditions
title_short Evolution of thermal and mechanical properties of Nitinol wire as a function of ageing treatment conditions
title_sort evolution of thermal and mechanical properties of nitinol wire as a function of ageing treatment conditions
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AT everaertsj evolutionofthermalandmechanicalpropertiesofnitinolwireasafunctionofageingtreatmentconditions
AT salvatie evolutionofthermalandmechanicalpropertiesofnitinolwireasafunctionofageingtreatmentconditions
AT korsunskya evolutionofthermalandmechanicalpropertiesofnitinolwireasafunctionofageingtreatmentconditions