Crystal nucleation in metallic alloys using x-ray radiography and machine learning

The crystallization of solidifying Al-Cu alloys over a wide range of conditions was studied in situ by synchrotron x-ray radiography, and the data were analyzed using a computer vision algorithm trained using machine learning. The effect of cooling rate and solute concentration on nucleation underco...

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Main Authors: Liotti, E, Arteta, C, Zisserman, A, Lui, A, Lempitsky, V, Grant, P
Format: Journal article
Language:English
Published: American Association for the Advancement of Science 2018
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author Liotti, E
Arteta, C
Zisserman, A
Lui, A
Lempitsky, V
Grant, P
author_facet Liotti, E
Arteta, C
Zisserman, A
Lui, A
Lempitsky, V
Grant, P
author_sort Liotti, E
collection OXFORD
description The crystallization of solidifying Al-Cu alloys over a wide range of conditions was studied in situ by synchrotron x-ray radiography, and the data were analyzed using a computer vision algorithm trained using machine learning. The effect of cooling rate and solute concentration on nucleation undercooling, crystal formation rate, and crystal growth rate was measured automatically for thousands of separate crystals, which was impossible to achieve manually. Nucleation undercooling distributions confirmed the efficiency of extrinsic grain refiners and gave support to the widely assumed free growth model of heterogeneous nucleation. We show that crystallization occurred in temporal and spatial bursts associated with a solute-suppressed nucleation zone.
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spelling oxford-uuid:47f7f437-94d9-43a9-b819-8d960994dfb92022-03-26T15:23:02ZCrystal nucleation in metallic alloys using x-ray radiography and machine learningJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:47f7f437-94d9-43a9-b819-8d960994dfb9EnglishSymplectic Elements at OxfordAmerican Association for the Advancement of Science2018Liotti, EArteta, CZisserman, ALui, ALempitsky, VGrant, PThe crystallization of solidifying Al-Cu alloys over a wide range of conditions was studied in situ by synchrotron x-ray radiography, and the data were analyzed using a computer vision algorithm trained using machine learning. The effect of cooling rate and solute concentration on nucleation undercooling, crystal formation rate, and crystal growth rate was measured automatically for thousands of separate crystals, which was impossible to achieve manually. Nucleation undercooling distributions confirmed the efficiency of extrinsic grain refiners and gave support to the widely assumed free growth model of heterogeneous nucleation. We show that crystallization occurred in temporal and spatial bursts associated with a solute-suppressed nucleation zone.
spellingShingle Liotti, E
Arteta, C
Zisserman, A
Lui, A
Lempitsky, V
Grant, P
Crystal nucleation in metallic alloys using x-ray radiography and machine learning
title Crystal nucleation in metallic alloys using x-ray radiography and machine learning
title_full Crystal nucleation in metallic alloys using x-ray radiography and machine learning
title_fullStr Crystal nucleation in metallic alloys using x-ray radiography and machine learning
title_full_unstemmed Crystal nucleation in metallic alloys using x-ray radiography and machine learning
title_short Crystal nucleation in metallic alloys using x-ray radiography and machine learning
title_sort crystal nucleation in metallic alloys using x ray radiography and machine learning
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AT luia crystalnucleationinmetallicalloysusingxrayradiographyandmachinelearning
AT lempitskyv crystalnucleationinmetallicalloysusingxrayradiographyandmachinelearning
AT grantp crystalnucleationinmetallicalloysusingxrayradiographyandmachinelearning