N,N'-bis(4-iodophenyl)diazene N-oxide
The synthesis of C 12H 8I 2N 2O, an unexpected product, obtained while converting N,N-dibutyl-4-iodoaniline into its N-oxide, was presented. A mixture of N,N-dibutyl-4-iodoaniline, chloroform, methanol, a...
| Main Authors: | , , , |
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| Format: | Journal article |
| Language: | English |
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2003
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| _version_ | 1797067538854576128 |
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| author | Krivokapic, A Wilson, C Watkin, D Anderson, H |
| author_facet | Krivokapic, A Wilson, C Watkin, D Anderson, H |
| author_sort | Krivokapic, A |
| collection | OXFORD |
| description | The synthesis of C 12H 8I 2N 2O, an unexpected product, obtained while converting N,N-dibutyl-4-iodoaniline into its N-oxide, was presented. A mixture of N,N-dibutyl-4-iodoaniline, chloroform, methanol, and hydrogen peroxide was heated to reflux. Until the starting material was fully consumed, the addition of hydrogen peroxide was continued. The product was then isolated, and allowed to get crystallized into colourless crystals. The product was found to crystrallize as a layer structure. |
| first_indexed | 2024-03-06T21:57:45Z |
| format | Journal article |
| id | oxford-uuid:4d812f3d-5004-471e-80f2-769249e845be |
| institution | University of Oxford |
| language | English |
| last_indexed | 2024-03-06T21:57:45Z |
| publishDate | 2003 |
| record_format | dspace |
| spelling | oxford-uuid:4d812f3d-5004-471e-80f2-769249e845be2022-03-26T15:55:49ZN,N'-bis(4-iodophenyl)diazene N-oxideJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:4d812f3d-5004-471e-80f2-769249e845beEnglishSymplectic Elements at Oxford2003Krivokapic, AWilson, CWatkin, DAnderson, HThe synthesis of C 12H 8I 2N 2O, an unexpected product, obtained while converting N,N-dibutyl-4-iodoaniline into its N-oxide, was presented. A mixture of N,N-dibutyl-4-iodoaniline, chloroform, methanol, and hydrogen peroxide was heated to reflux. Until the starting material was fully consumed, the addition of hydrogen peroxide was continued. The product was then isolated, and allowed to get crystallized into colourless crystals. The product was found to crystrallize as a layer structure. |
| spellingShingle | Krivokapic, A Wilson, C Watkin, D Anderson, H N,N'-bis(4-iodophenyl)diazene N-oxide |
| title | N,N'-bis(4-iodophenyl)diazene N-oxide |
| title_full | N,N'-bis(4-iodophenyl)diazene N-oxide |
| title_fullStr | N,N'-bis(4-iodophenyl)diazene N-oxide |
| title_full_unstemmed | N,N'-bis(4-iodophenyl)diazene N-oxide |
| title_short | N,N'-bis(4-iodophenyl)diazene N-oxide |
| title_sort | n n bis 4 iodophenyl diazene n oxide |
| work_keys_str_mv | AT krivokapica nnbis4iodophenyldiazenenoxide AT wilsonc nnbis4iodophenyldiazenenoxide AT watkind nnbis4iodophenyldiazenenoxide AT andersonh nnbis4iodophenyldiazenenoxide |