Indium hydroxide and indium oxide nanospheres, nanoflowers, microcubes, and nanorods: Synthesis and optical properties

This paper reports the facile synthesis of indium hydroxide nanospheres, nanoflowers, microcubes, and nanorods using a solvothermal method at 240 °C for 18 h in an ethanol solution of indium acetate with the directing surfactants of ethylenediamine, acetic acid, and oleic acid. After calcination of...

Full description

Bibliographic Details
Main Authors: Du, J, Yang, M, Cha, S, Rhen, D, Kang, M, Kang, D
Format: Journal article
Language:English
Published: 2008
_version_ 1826274740768079872
author Du, J
Yang, M
Cha, S
Rhen, D
Kang, M
Kang, D
author_facet Du, J
Yang, M
Cha, S
Rhen, D
Kang, M
Kang, D
author_sort Du, J
collection OXFORD
description This paper reports the facile synthesis of indium hydroxide nanospheres, nanoflowers, microcubes, and nanorods using a solvothermal method at 240 °C for 18 h in an ethanol solution of indium acetate with the directing surfactants of ethylenediamine, acetic acid, and oleic acid. After calcination of as-synthesized indium hydroxide products at 500 °C for 4 h, corresponding indium oxide nanostructures were also obtained with sizes and morphologies similar to the indium hydroxide products. The phase compositions and morphologies of the resulting samples were characterized by X-ray diffraction, Raman spectroscopy, scanning electron microscopy, transmission electron microscopy, and selected area electron diffraction. On the basis of our findings, we propose a surfactant-assisted self-assembly formation mechanism to account for their formation processes. Room temperature photoluminescence was further carried out on the indium oxide samples to investigate their optical properties. © 2008 American Chemical Society.
first_indexed 2024-03-06T22:48:03Z
format Journal article
id oxford-uuid:5dddb4b2-3093-418d-9f23-ad506e45e292
institution University of Oxford
language English
last_indexed 2024-03-06T22:48:03Z
publishDate 2008
record_format dspace
spelling oxford-uuid:5dddb4b2-3093-418d-9f23-ad506e45e2922022-03-26T17:36:56ZIndium hydroxide and indium oxide nanospheres, nanoflowers, microcubes, and nanorods: Synthesis and optical propertiesJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:5dddb4b2-3093-418d-9f23-ad506e45e292EnglishSymplectic Elements at Oxford2008Du, JYang, MCha, SRhen, DKang, MKang, DThis paper reports the facile synthesis of indium hydroxide nanospheres, nanoflowers, microcubes, and nanorods using a solvothermal method at 240 °C for 18 h in an ethanol solution of indium acetate with the directing surfactants of ethylenediamine, acetic acid, and oleic acid. After calcination of as-synthesized indium hydroxide products at 500 °C for 4 h, corresponding indium oxide nanostructures were also obtained with sizes and morphologies similar to the indium hydroxide products. The phase compositions and morphologies of the resulting samples were characterized by X-ray diffraction, Raman spectroscopy, scanning electron microscopy, transmission electron microscopy, and selected area electron diffraction. On the basis of our findings, we propose a surfactant-assisted self-assembly formation mechanism to account for their formation processes. Room temperature photoluminescence was further carried out on the indium oxide samples to investigate their optical properties. © 2008 American Chemical Society.
spellingShingle Du, J
Yang, M
Cha, S
Rhen, D
Kang, M
Kang, D
Indium hydroxide and indium oxide nanospheres, nanoflowers, microcubes, and nanorods: Synthesis and optical properties
title Indium hydroxide and indium oxide nanospheres, nanoflowers, microcubes, and nanorods: Synthesis and optical properties
title_full Indium hydroxide and indium oxide nanospheres, nanoflowers, microcubes, and nanorods: Synthesis and optical properties
title_fullStr Indium hydroxide and indium oxide nanospheres, nanoflowers, microcubes, and nanorods: Synthesis and optical properties
title_full_unstemmed Indium hydroxide and indium oxide nanospheres, nanoflowers, microcubes, and nanorods: Synthesis and optical properties
title_short Indium hydroxide and indium oxide nanospheres, nanoflowers, microcubes, and nanorods: Synthesis and optical properties
title_sort indium hydroxide and indium oxide nanospheres nanoflowers microcubes and nanorods synthesis and optical properties
work_keys_str_mv AT duj indiumhydroxideandindiumoxidenanospheresnanoflowersmicrocubesandnanorodssynthesisandopticalproperties
AT yangm indiumhydroxideandindiumoxidenanospheresnanoflowersmicrocubesandnanorodssynthesisandopticalproperties
AT chas indiumhydroxideandindiumoxidenanospheresnanoflowersmicrocubesandnanorodssynthesisandopticalproperties
AT rhend indiumhydroxideandindiumoxidenanospheresnanoflowersmicrocubesandnanorodssynthesisandopticalproperties
AT kangm indiumhydroxideandindiumoxidenanospheresnanoflowersmicrocubesandnanorodssynthesisandopticalproperties
AT kangd indiumhydroxideandindiumoxidenanospheresnanoflowersmicrocubesandnanorodssynthesisandopticalproperties