APPARATUS FOR THE IN-SITU KINETIC-STUDY OF REACTIONS INVOLVING AIR SENSITIVE MATERIALS USING ENERGY-DISPERSIVE POWER DIFFRACTION

A novel sample chamber has been developed for the study of chemical reactions involving air sensitive samples using energy-dispersive powder diffraction. The apparatus consists of a reaction vessel, automatic reactant dispensing system, heating jacket, stirrer, and gas purge system. The use of this...

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Bibliographic Details
Main Authors: Clark, S, Irvin, P, Flaherty, J, Rathbone, T, Wong, H, Evans, J, Ohare, D
Format: Journal article
Language:English
Published: 1994
Description
Summary:A novel sample chamber has been developed for the study of chemical reactions involving air sensitive samples using energy-dispersive powder diffraction. The apparatus consists of a reaction vessel, automatic reactant dispensing system, heating jacket, stirrer, and gas purge system. The use of this apparatus is illustrated with data collected on station 9.7 of the UK Synchrotron Radiation Source during a study on the intercalation of cobaltocene into tin disulfide.