Tetragonality of Fe-C martensite – a pattern matching electron backscatter diffraction analysis compared to X-ray diffraction
Measurements of the local tetragonality in Fe-C martensite at microstructural length-scale through pattern matching of electron backscatter diffraction patterns (EBSPs) and careful calibration of detector geometry are presented. It is found that the local tetragonality varies within the complex micr...
| Main Authors: | , , , |
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| Format: | Journal article |
| Language: | English |
| Published: |
Elsevier
2020
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| _version_ | 1797077803013767168 |
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| author | Tanaka, T Maruyama, N Nakamura, N Wilkinson, AJ |
| author_facet | Tanaka, T Maruyama, N Nakamura, N Wilkinson, AJ |
| author_sort | Tanaka, T |
| collection | OXFORD |
| description | Measurements of the local tetragonality in Fe-C martensite at microstructural
length-scale through pattern matching of electron backscatter diffraction
patterns (EBSPs) and careful calibration of detector geometry are presented. It
is found that the local tetragonality varies within the complex microstructure
by several per cent at largest and that the scatter in the axial ratio is
increased at higher nominal carbon content. At some analysis points the local
crystal structure can be regarded as lower symmetry than simple body centred
tetragonal. A linear relation between the nominal carbon content and averaged
local tetragonality measured by EBSD is also obtained, although the averaged
axial ratio is slightly below that obtained from more classical X-ray
diffraction measurements. |
| first_indexed | 2024-03-07T00:23:14Z |
| format | Journal article |
| id | oxford-uuid:7d408003-7c17-43c4-a2dd-64deb4d65c4c |
| institution | University of Oxford |
| language | English |
| last_indexed | 2024-03-07T00:23:14Z |
| publishDate | 2020 |
| publisher | Elsevier |
| record_format | dspace |
| spelling | oxford-uuid:7d408003-7c17-43c4-a2dd-64deb4d65c4c2022-03-26T21:02:24ZTetragonality of Fe-C martensite – a pattern matching electron backscatter diffraction analysis compared to X-ray diffractionJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:7d408003-7c17-43c4-a2dd-64deb4d65c4cEnglishSymplectic ElementsElsevier 2020Tanaka, TMaruyama, NNakamura, NWilkinson, AJMeasurements of the local tetragonality in Fe-C martensite at microstructural length-scale through pattern matching of electron backscatter diffraction patterns (EBSPs) and careful calibration of detector geometry are presented. It is found that the local tetragonality varies within the complex microstructure by several per cent at largest and that the scatter in the axial ratio is increased at higher nominal carbon content. At some analysis points the local crystal structure can be regarded as lower symmetry than simple body centred tetragonal. A linear relation between the nominal carbon content and averaged local tetragonality measured by EBSD is also obtained, although the averaged axial ratio is slightly below that obtained from more classical X-ray diffraction measurements. |
| spellingShingle | Tanaka, T Maruyama, N Nakamura, N Wilkinson, AJ Tetragonality of Fe-C martensite – a pattern matching electron backscatter diffraction analysis compared to X-ray diffraction |
| title | Tetragonality of Fe-C martensite – a pattern matching electron backscatter diffraction analysis compared to X-ray diffraction |
| title_full | Tetragonality of Fe-C martensite – a pattern matching electron backscatter diffraction analysis compared to X-ray diffraction |
| title_fullStr | Tetragonality of Fe-C martensite – a pattern matching electron backscatter diffraction analysis compared to X-ray diffraction |
| title_full_unstemmed | Tetragonality of Fe-C martensite – a pattern matching electron backscatter diffraction analysis compared to X-ray diffraction |
| title_short | Tetragonality of Fe-C martensite – a pattern matching electron backscatter diffraction analysis compared to X-ray diffraction |
| title_sort | tetragonality of fe c martensite a pattern matching electron backscatter diffraction analysis compared to x ray diffraction |
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