The concomitant crystallization of two polymorphs of 1-deoxy-alpha-D-tagatose.
The crystalline form of 1-deoxy-D-tagatose, C6H12O5, is shown to be 1-deoxy-alpha-D-tagatopyranose; the absolute configuration is determined by use of D-lyxono-1,4-lactone as the starting material. The title compound crystallized as concomitant polymorphs from a mixture of ethyl actate and methanol....
| Prif Awduron: | , , , , , |
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| Fformat: | Journal article |
| Iaith: | English |
| Cyhoeddwyd: |
2007
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| _version_ | 1826281416908865536 |
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| author | Jones, N Jenkinson, S Soengas, R Izumori, K Fleet, G Watkin, D |
| author_facet | Jones, N Jenkinson, S Soengas, R Izumori, K Fleet, G Watkin, D |
| author_sort | Jones, N |
| collection | OXFORD |
| description | The crystalline form of 1-deoxy-D-tagatose, C6H12O5, is shown to be 1-deoxy-alpha-D-tagatopyranose; the absolute configuration is determined by use of D-lyxono-1,4-lactone as the starting material. The title compound crystallized as concomitant polymorphs from a mixture of ethyl actate and methanol. Although the melting points of the materials differ by 7 K, the molecular conformations are almost identical and, in both polymorphs, each molecule is subject to four O-H...O hydrogen bonds. |
| first_indexed | 2024-03-07T00:28:29Z |
| format | Journal article |
| id | oxford-uuid:7ef21e7e-8efe-4e43-b92d-a69b2eea2a9d |
| institution | University of Oxford |
| language | English |
| last_indexed | 2024-03-07T00:28:29Z |
| publishDate | 2007 |
| record_format | dspace |
| spelling | oxford-uuid:7ef21e7e-8efe-4e43-b92d-a69b2eea2a9d2022-03-26T21:13:31ZThe concomitant crystallization of two polymorphs of 1-deoxy-alpha-D-tagatose.Journal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:7ef21e7e-8efe-4e43-b92d-a69b2eea2a9dEnglishSymplectic Elements at Oxford2007Jones, NJenkinson, SSoengas, RIzumori, KFleet, GWatkin, DThe crystalline form of 1-deoxy-D-tagatose, C6H12O5, is shown to be 1-deoxy-alpha-D-tagatopyranose; the absolute configuration is determined by use of D-lyxono-1,4-lactone as the starting material. The title compound crystallized as concomitant polymorphs from a mixture of ethyl actate and methanol. Although the melting points of the materials differ by 7 K, the molecular conformations are almost identical and, in both polymorphs, each molecule is subject to four O-H...O hydrogen bonds. |
| spellingShingle | Jones, N Jenkinson, S Soengas, R Izumori, K Fleet, G Watkin, D The concomitant crystallization of two polymorphs of 1-deoxy-alpha-D-tagatose. |
| title | The concomitant crystallization of two polymorphs of 1-deoxy-alpha-D-tagatose. |
| title_full | The concomitant crystallization of two polymorphs of 1-deoxy-alpha-D-tagatose. |
| title_fullStr | The concomitant crystallization of two polymorphs of 1-deoxy-alpha-D-tagatose. |
| title_full_unstemmed | The concomitant crystallization of two polymorphs of 1-deoxy-alpha-D-tagatose. |
| title_short | The concomitant crystallization of two polymorphs of 1-deoxy-alpha-D-tagatose. |
| title_sort | concomitant crystallization of two polymorphs of 1 deoxy alpha d tagatose |
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