Voltammetric sizing of a sphere.
The size of a glass sphere positioned in the center of a microdisk electrode is determined by using a simple electrochemical procedure and is confirmed, additionally, by a microscopical measurement of the sphere at the time of the electrochemical measurement. The cyclic voltammetric response of the...
| Hauptverfasser: | , , , , |
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| Format: | Journal article |
| Sprache: | English |
| Veröffentlicht: |
2006
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| _version_ | 1826286135506108416 |
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| author | Fietkau, N Chevallier, F Jiang, L Jones, T Compton, R |
| author_facet | Fietkau, N Chevallier, F Jiang, L Jones, T Compton, R |
| author_sort | Fietkau, N |
| collection | OXFORD |
| description | The size of a glass sphere positioned in the center of a microdisk electrode is determined by using a simple electrochemical procedure and is confirmed, additionally, by a microscopical measurement of the sphere at the time of the electrochemical measurement. The cyclic voltammetric response of the naked electrode and of the electrode with the sphere positioned in its center is recorded over a wide range of scan rates (0.002-1.5 V s(-1)). The size of the sphere is then determined by comparison of the experimental voltammogram with simulations for each individual scan rate. |
| first_indexed | 2024-03-07T01:39:17Z |
| format | Journal article |
| id | oxford-uuid:964bb1d3-c9c4-449e-992e-ff105ebb755f |
| institution | University of Oxford |
| language | English |
| last_indexed | 2024-03-07T01:39:17Z |
| publishDate | 2006 |
| record_format | dspace |
| spelling | oxford-uuid:964bb1d3-c9c4-449e-992e-ff105ebb755f2022-03-26T23:51:57ZVoltammetric sizing of a sphere.Journal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:964bb1d3-c9c4-449e-992e-ff105ebb755fEnglishSymplectic Elements at Oxford2006Fietkau, NChevallier, FJiang, LJones, TCompton, RThe size of a glass sphere positioned in the center of a microdisk electrode is determined by using a simple electrochemical procedure and is confirmed, additionally, by a microscopical measurement of the sphere at the time of the electrochemical measurement. The cyclic voltammetric response of the naked electrode and of the electrode with the sphere positioned in its center is recorded over a wide range of scan rates (0.002-1.5 V s(-1)). The size of the sphere is then determined by comparison of the experimental voltammogram with simulations for each individual scan rate. |
| spellingShingle | Fietkau, N Chevallier, F Jiang, L Jones, T Compton, R Voltammetric sizing of a sphere. |
| title | Voltammetric sizing of a sphere. |
| title_full | Voltammetric sizing of a sphere. |
| title_fullStr | Voltammetric sizing of a sphere. |
| title_full_unstemmed | Voltammetric sizing of a sphere. |
| title_short | Voltammetric sizing of a sphere. |
| title_sort | voltammetric sizing of a sphere |
| work_keys_str_mv | AT fietkaun voltammetricsizingofasphere AT chevallierf voltammetricsizingofasphere AT jiangl voltammetricsizingofasphere AT jonest voltammetricsizingofasphere AT comptonr voltammetricsizingofasphere |