SYNTHESES OF [2-C-13] AND [1,2-C-13] LABELED ALPHA-KETOGLUTARIC ACID
The syntheses of α-keto[2-13C]glutaric acid and α-keto[1,2-13C]glutaric acid were each achieved from commercial 13CH3I in 5 steps. 13CH3NO2, prepared in situ from 13CH3I and AgNO2, was treated with magnesium methyl carbonate, followed by acidified methanol to give O2N13CH2CO2CH3. Michael addition to...
| Main Authors: | , , , , |
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| Format: | Journal article |
| Language: | English |
| Published: |
1989
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