A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell
An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-reso...
| Main Authors: | , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , , |
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| Format: | Journal article |
| Language: | English |
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International Union of Crystallography
2023
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| _version_ | 1826310831647752192 |
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| author | Husband, RJ Strohm, C Appel, K Ball, OB Briggs, R Buchen, J Cerantola, V Chariton, S Coleman, AL Cynn, H Dattelbaum, D Dwivedi, A Eggert, JH Ehm, L Evans, WJ Glazyrin, K Goncharov, AF Graafsma, H Howard, A Huston, L Hutchinson, TM Hwang, H Jacob, S Kaa, J Kim, J Kim, M Koemets, E Konôpková, Z Langenhorst, F Laurus, T Li, X Mainberger, J Marquardt, H McBride, EE McGuire, C McHardy, JD McMahon, MI McWilliams, RS Méndez, ASJ Mondal, A Morard, G O'Bannon, EF Otzen, C Pépin, CM Prakapenka, VB Prescher, C Preston, TR Redmer, R Roeper, M Sanchez-Valle, C |
| author_facet | Husband, RJ Strohm, C Appel, K Ball, OB Briggs, R Buchen, J Cerantola, V Chariton, S Coleman, AL Cynn, H Dattelbaum, D Dwivedi, A Eggert, JH Ehm, L Evans, WJ Glazyrin, K Goncharov, AF Graafsma, H Howard, A Huston, L Hutchinson, TM Hwang, H Jacob, S Kaa, J Kim, J Kim, M Koemets, E Konôpková, Z Langenhorst, F Laurus, T Li, X Mainberger, J Marquardt, H McBride, EE McGuire, C McHardy, JD McMahon, MI McWilliams, RS Méndez, ASJ Mondal, A Morard, G O'Bannon, EF Otzen, C Pépin, CM Prakapenka, VB Prescher, C Preston, TR Redmer, R Roeper, M Sanchez-Valle, C |
| author_sort | Husband, RJ |
| collection | OXFORD |
| description | An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1. |
| first_indexed | 2024-03-07T07:59:20Z |
| format | Journal article |
| id | oxford-uuid:a51914ac-409e-4ee6-9d40-1f1b00889cfc |
| institution | University of Oxford |
| language | English |
| last_indexed | 2024-03-07T07:59:20Z |
| publishDate | 2023 |
| publisher | International Union of Crystallography |
| record_format | dspace |
| spelling | oxford-uuid:a51914ac-409e-4ee6-9d40-1f1b00889cfc2023-09-12T15:45:35ZA MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cellJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:a51914ac-409e-4ee6-9d40-1f1b00889cfcEnglishSymplectic ElementsInternational Union of Crystallography2023Husband, RJStrohm, CAppel, KBall, OBBriggs, RBuchen, JCerantola, VChariton, SColeman, ALCynn, HDattelbaum, DDwivedi, AEggert, JHEhm, LEvans, WJGlazyrin, KGoncharov, AFGraafsma, HHoward, AHuston, LHutchinson, TMHwang, HJacob, SKaa, JKim, JKim, MKoemets, EKonôpková, ZLangenhorst, FLaurus, TLi, XMainberger, JMarquardt, HMcBride, EEMcGuire, CMcHardy, JDMcMahon, MIMcWilliams, RSMéndez, ASJMondal, AMorard, GO'Bannon, EFOtzen, CPépin, CMPrakapenka, VBPrescher, CPreston, TRRedmer, RRoeper, MSanchez-Valle, CAn experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1. |
| spellingShingle | Husband, RJ Strohm, C Appel, K Ball, OB Briggs, R Buchen, J Cerantola, V Chariton, S Coleman, AL Cynn, H Dattelbaum, D Dwivedi, A Eggert, JH Ehm, L Evans, WJ Glazyrin, K Goncharov, AF Graafsma, H Howard, A Huston, L Hutchinson, TM Hwang, H Jacob, S Kaa, J Kim, J Kim, M Koemets, E Konôpková, Z Langenhorst, F Laurus, T Li, X Mainberger, J Marquardt, H McBride, EE McGuire, C McHardy, JD McMahon, MI McWilliams, RS Méndez, ASJ Mondal, A Morard, G O'Bannon, EF Otzen, C Pépin, CM Prakapenka, VB Prescher, C Preston, TR Redmer, R Roeper, M Sanchez-Valle, C A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_full | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_fullStr | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_full_unstemmed | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_short | A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell |
| title_sort | mhz x ray diffraction set up for dynamic compression experiments in the diamond anvil cell |
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