An investigation of weak CH...O hydrogen bonds in maltose anomers by a combination of calculation and experimental solid-state NMR spectroscopy.
Two-dimensional (1)H-(13)C MAS-J-HMQC solid-state NMR spectra of the two anomeric forms of maltose at natural abundance are presented. The experimental (1)H chemical shifts of the CH and CH(2) protons are assigned using first-principles chemical shift calculations that employ a plane-wave pseudopote...
Main Authors: | Yates, JR, Pham, T, Pickard, C, Mauri, F, Amado, A, Gil, A, Brown, S |
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Format: | Journal article |
Language: | English |
Published: |
2005
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