A gas-phase reaction cell for modern Atom Probe systems

In this work, we demonstrate a new system for the examination of gas interactions with surfaces via Atom Probe Tomography. This system provides the capability to examine the surface and subsurface interactions of gases with a wide range of specimens, as well as a selection of input gas types. This s...

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Main Authors: Haley, D, McCarrol, I, Bagot, P, Cairney, J, Moody, M
Format: Journal article
Published: Cambridge University Press 2019
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author Haley, D
McCarrol, I
Bagot, P
Cairney, J
Moody, M
author_facet Haley, D
McCarrol, I
Bagot, P
Cairney, J
Moody, M
author_sort Haley, D
collection OXFORD
description In this work, we demonstrate a new system for the examination of gas interactions with surfaces via Atom Probe Tomography. This system provides the capability to examine the surface and subsurface interactions of gases with a wide range of specimens, as well as a selection of input gas types. This system has been primarily developed to aid the investigation of hydrogen interactions with metallurgical samples, to better understand the phenomenon of hydrogen embrittlement. In its current form, it is able to operate at pressures from 10􀀀6 to 1000 mbar (abs), can operate using a variety of gasses, and is equipped with heating and cryogenic quenching capabilities. We use this system to examine the interaction of hydrogen with Pd, as well as the interaction of water vapour and oxygen in Mg samples.
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spelling oxford-uuid:c9536397-227b-41ba-8f26-3af689adaa432022-03-27T06:58:22ZA gas-phase reaction cell for modern Atom Probe systemsJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:c9536397-227b-41ba-8f26-3af689adaa43Symplectic Elements at OxfordCambridge University Press2019Haley, DMcCarrol, IBagot, PCairney, JMoody, MIn this work, we demonstrate a new system for the examination of gas interactions with surfaces via Atom Probe Tomography. This system provides the capability to examine the surface and subsurface interactions of gases with a wide range of specimens, as well as a selection of input gas types. This system has been primarily developed to aid the investigation of hydrogen interactions with metallurgical samples, to better understand the phenomenon of hydrogen embrittlement. In its current form, it is able to operate at pressures from 10􀀀6 to 1000 mbar (abs), can operate using a variety of gasses, and is equipped with heating and cryogenic quenching capabilities. We use this system to examine the interaction of hydrogen with Pd, as well as the interaction of water vapour and oxygen in Mg samples.
spellingShingle Haley, D
McCarrol, I
Bagot, P
Cairney, J
Moody, M
A gas-phase reaction cell for modern Atom Probe systems
title A gas-phase reaction cell for modern Atom Probe systems
title_full A gas-phase reaction cell for modern Atom Probe systems
title_fullStr A gas-phase reaction cell for modern Atom Probe systems
title_full_unstemmed A gas-phase reaction cell for modern Atom Probe systems
title_short A gas-phase reaction cell for modern Atom Probe systems
title_sort gas phase reaction cell for modern atom probe systems
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AT mccarroli agasphasereactioncellformodernatomprobesystems
AT bagotp agasphasereactioncellformodernatomprobesystems
AT cairneyj agasphasereactioncellformodernatomprobesystems
AT moodym agasphasereactioncellformodernatomprobesystems
AT haleyd gasphasereactioncellformodernatomprobesystems
AT mccarroli gasphasereactioncellformodernatomprobesystems
AT bagotp gasphasereactioncellformodernatomprobesystems
AT cairneyj gasphasereactioncellformodernatomprobesystems
AT moodym gasphasereactioncellformodernatomprobesystems