Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction
The design and use of a pressure cell for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction are described. This novel apparatus allows the kinetics and mechanism of the crystallization of complex inorganic solids, such as zeolites and other microporous materi...
| Main Authors: | , , , , , , |
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| פורמט: | Journal article |
| שפה: | English |
| יצא לאור: |
1999
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| _version_ | 1826297661620224000 |
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| author | Walton, R Francis, R Halasyamani, P O' Hare, D Smith, R Done, R Humphreys, R |
| author_facet | Walton, R Francis, R Halasyamani, P O' Hare, D Smith, R Done, R Humphreys, R |
| author_sort | Walton, R |
| collection | OXFORD |
| description | The design and use of a pressure cell for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction are described. This novel apparatus allows the kinetics and mechanism of the crystallization of complex inorganic solids, such as zeolites and other microporous materials, to be investigated under laboratory conditions. Reactions can be studied over a wide range of temperatures (25-250 °C) under conditions of autogenous pressure (1-22 bar). The use of the cell is demonstrated by a study of the hydrothermal crystallization of the zeolite sodium hydroxosodalite with time-of-flight neutron diffraction data collected using the Polaris diffractometer of the United Kingdom's pulsed spallation neutron source, ISIS. © 1999 American Institute of Physics. |
| first_indexed | 2024-03-07T04:35:04Z |
| format | Journal article |
| id | oxford-uuid:cfa64596-93b5-4a7f-a869-d1f5eea35767 |
| institution | University of Oxford |
| language | English |
| last_indexed | 2024-03-07T04:35:04Z |
| publishDate | 1999 |
| record_format | dspace |
| spelling | oxford-uuid:cfa64596-93b5-4a7f-a869-d1f5eea357672022-03-27T07:44:13ZNovel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffractionJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:cfa64596-93b5-4a7f-a869-d1f5eea35767EnglishSymplectic Elements at Oxford1999Walton, RFrancis, RHalasyamani, PO' Hare, DSmith, RDone, RHumphreys, RThe design and use of a pressure cell for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction are described. This novel apparatus allows the kinetics and mechanism of the crystallization of complex inorganic solids, such as zeolites and other microporous materials, to be investigated under laboratory conditions. Reactions can be studied over a wide range of temperatures (25-250 °C) under conditions of autogenous pressure (1-22 bar). The use of the cell is demonstrated by a study of the hydrothermal crystallization of the zeolite sodium hydroxosodalite with time-of-flight neutron diffraction data collected using the Polaris diffractometer of the United Kingdom's pulsed spallation neutron source, ISIS. © 1999 American Institute of Physics. |
| spellingShingle | Walton, R Francis, R Halasyamani, P O' Hare, D Smith, R Done, R Humphreys, R Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction |
| title | Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction |
| title_full | Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction |
| title_fullStr | Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction |
| title_full_unstemmed | Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction |
| title_short | Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction |
| title_sort | novel apparatus for the in situ study of hydrothermal crystallizations using time resolved neutron diffraction |
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