Microstructural characterization of YO ODS-Fe-Cr model alloys

Two Fe-12 wt% Cr alloys, one containing 0.4 wt% YO and the other YO-free, have been produced by mechanical alloying followed by hot isostatic pressing. These oxide dispersion strengthened and reference alloys were characterized both in the as-HIPed state and after tempering by transmission electron...

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Main Authors: de Castro, V, Marquis, E, Lozano-Perez, S, Jenkins, M, Leguey, T, Muñoz, A, Monge, M, Pareja, R
Format: Journal article
Published: 2009
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author de Castro, V
Marquis, E
Lozano-Perez, S
Jenkins, M
Leguey, T
Muñoz, A
Monge, M
Pareja, R
author_facet de Castro, V
Marquis, E
Lozano-Perez, S
Jenkins, M
Leguey, T
Muñoz, A
Monge, M
Pareja, R
author_sort de Castro, V
collection OXFORD
description Two Fe-12 wt% Cr alloys, one containing 0.4 wt% YO and the other YO-free, have been produced by mechanical alloying followed by hot isostatic pressing. These oxide dispersion strengthened and reference alloys were characterized both in the as-HIPed state and after tempering by transmission electron microscopy and atom-probe tomography. The as-HIPed alloys exhibited the characteristic microstructure of lath martensite and contained a high density of dislocations. Small voids with sizes <10 nm were also observed. Both alloys also contained MC and MC carbides (M = Cr, Fe) probably as a result of C ingress during milling. After tempering at 1023 K for 4 h the microstructures had partially recovered. In the recovered regions, martensite laths were replaced by equiaxed grains in which MC carbides decorated the grain boundaries. In the ODS alloy nanoparticles containing Y were commonly observed within grains, although they were also present at grain boundaries and adjacent to large carbides. © 2009 Elsevier B.V. All rights reserved.
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spelling oxford-uuid:e4af3f3e-a9c7-442c-8fec-a05a50d24ae12022-03-27T10:18:22ZMicrostructural characterization of YO ODS-Fe-Cr model alloysJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:e4af3f3e-a9c7-442c-8fec-a05a50d24ae1Symplectic Elements at Oxford2009de Castro, VMarquis, ELozano-Perez, SJenkins, MLeguey, TMuñoz, AMonge, MPareja, RTwo Fe-12 wt% Cr alloys, one containing 0.4 wt% YO and the other YO-free, have been produced by mechanical alloying followed by hot isostatic pressing. These oxide dispersion strengthened and reference alloys were characterized both in the as-HIPed state and after tempering by transmission electron microscopy and atom-probe tomography. The as-HIPed alloys exhibited the characteristic microstructure of lath martensite and contained a high density of dislocations. Small voids with sizes <10 nm were also observed. Both alloys also contained MC and MC carbides (M = Cr, Fe) probably as a result of C ingress during milling. After tempering at 1023 K for 4 h the microstructures had partially recovered. In the recovered regions, martensite laths were replaced by equiaxed grains in which MC carbides decorated the grain boundaries. In the ODS alloy nanoparticles containing Y were commonly observed within grains, although they were also present at grain boundaries and adjacent to large carbides. © 2009 Elsevier B.V. All rights reserved.
spellingShingle de Castro, V
Marquis, E
Lozano-Perez, S
Jenkins, M
Leguey, T
Muñoz, A
Monge, M
Pareja, R
Microstructural characterization of YO ODS-Fe-Cr model alloys
title Microstructural characterization of YO ODS-Fe-Cr model alloys
title_full Microstructural characterization of YO ODS-Fe-Cr model alloys
title_fullStr Microstructural characterization of YO ODS-Fe-Cr model alloys
title_full_unstemmed Microstructural characterization of YO ODS-Fe-Cr model alloys
title_short Microstructural characterization of YO ODS-Fe-Cr model alloys
title_sort microstructural characterization of yo ods fe cr model alloys
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