Enhancing resolution and sensitivity of O-17 solid-state NMR through combining double rotation, H-1 decoupling and satellite modulation for biomolecular applications
17O solid-state NMR is a highly sensitive probe of structural detail of organic solids but improvements in sensitivity and resolution are crucial for it to be applied to larger biological molecules. Here it is shown that high resolution (∼1 ppm) and significant signal enhancement can be achieved by...
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Bibliographic Details
Main Authors: |
Howes, A,
Anupold, T,
Lemaitre, V,
Kukol, A,
Watts, A,
Samoson, A,
Smith, M,
Dupree, R |
Format: | Journal article
|
Language: | English |
Published: |
2006
|