Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction

Precise channel-to-energy conversion is very important in full-pattern refinement in energy-dispersive X-ray diffraction. Careful examination shows that the channel-to-energy conversion is not entirely linear, which presents an obstacle to obtaining accurate quantitative data for lattice strains by...

Disgrifiad llawn

Manylion Llyfryddiaeth
Prif Awduron: Liu, J, Kim, K, Golshan, M, Laundy, D, Korsunsky, A
Fformat: Journal article
Iaith:English
Cyhoeddwyd: Wiley-Blackwell 2005
Pynciau:
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author Liu, J
Kim, K
Golshan, M
Laundy, D
Korsunsky, A
author_facet Liu, J
Kim, K
Golshan, M
Laundy, D
Korsunsky, A
author_sort Liu, J
collection OXFORD
description Precise channel-to-energy conversion is very important in full-pattern refinement in energy-dispersive X-ray diffraction. Careful examination shows that the channel-to-energy conversion is not entirely linear, which presents an obstacle to obtaining accurate quantitative data for lattice strains by pattern refinement. In order to establish an accurate quadratic channel-to-energy conversion function, a Matlab program was written to find the best quadratic coefficient and hence the whole energy conversion function. Then this energy conversion function was used to perform a whole-pattern fitting of the energy-dispersive X-ray diffraction pattern of a Ti64 sample. The strain across the Ti64 bar calculated from the fitting results has been compared with values obtained by single-wavelength X-ray diffraction utilizing a Laue monochromator. © 2005 International Union of Crystallography.
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spelling oxford-uuid:e7f2ab3e-3f5b-4207-9ef3-9f34ba074cf42022-03-27T10:42:55ZEnergy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffractionJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:e7f2ab3e-3f5b-4207-9ef3-9f34ba074cf4Engineering and allied sciencesEnglishSymplectic Elements at OxfordWiley-Blackwell2005Liu, JKim, KGolshan, MLaundy, DKorsunsky, APrecise channel-to-energy conversion is very important in full-pattern refinement in energy-dispersive X-ray diffraction. Careful examination shows that the channel-to-energy conversion is not entirely linear, which presents an obstacle to obtaining accurate quantitative data for lattice strains by pattern refinement. In order to establish an accurate quadratic channel-to-energy conversion function, a Matlab program was written to find the best quadratic coefficient and hence the whole energy conversion function. Then this energy conversion function was used to perform a whole-pattern fitting of the energy-dispersive X-ray diffraction pattern of a Ti64 sample. The strain across the Ti64 bar calculated from the fitting results has been compared with values obtained by single-wavelength X-ray diffraction utilizing a Laue monochromator. © 2005 International Union of Crystallography.
spellingShingle Engineering and allied sciences
Liu, J
Kim, K
Golshan, M
Laundy, D
Korsunsky, A
Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction
title Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction
title_full Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction
title_fullStr Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction
title_full_unstemmed Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction
title_short Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction
title_sort energy calibration and full pattern refinement for strain analysis using energy dispersive and monochromatic x ray diffraction
topic Engineering and allied sciences
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AT golshanm energycalibrationandfullpatternrefinementforstrainanalysisusingenergydispersiveandmonochromaticxraydiffraction
AT laundyd energycalibrationandfullpatternrefinementforstrainanalysisusingenergydispersiveandmonochromaticxraydiffraction
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