Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction
Precise channel-to-energy conversion is very important in full-pattern refinement in energy-dispersive X-ray diffraction. Careful examination shows that the channel-to-energy conversion is not entirely linear, which presents an obstacle to obtaining accurate quantitative data for lattice strains by...
Prif Awduron: | , , , , |
---|---|
Fformat: | Journal article |
Iaith: | English |
Cyhoeddwyd: |
Wiley-Blackwell
2005
|
Pynciau: |
_version_ | 1826302483459211264 |
---|---|
author | Liu, J Kim, K Golshan, M Laundy, D Korsunsky, A |
author_facet | Liu, J Kim, K Golshan, M Laundy, D Korsunsky, A |
author_sort | Liu, J |
collection | OXFORD |
description | Precise channel-to-energy conversion is very important in full-pattern refinement in energy-dispersive X-ray diffraction. Careful examination shows that the channel-to-energy conversion is not entirely linear, which presents an obstacle to obtaining accurate quantitative data for lattice strains by pattern refinement. In order to establish an accurate quadratic channel-to-energy conversion function, a Matlab program was written to find the best quadratic coefficient and hence the whole energy conversion function. Then this energy conversion function was used to perform a whole-pattern fitting of the energy-dispersive X-ray diffraction pattern of a Ti64 sample. The strain across the Ti64 bar calculated from the fitting results has been compared with values obtained by single-wavelength X-ray diffraction utilizing a Laue monochromator. © 2005 International Union of Crystallography. |
first_indexed | 2024-03-07T05:48:13Z |
format | Journal article |
id | oxford-uuid:e7f2ab3e-3f5b-4207-9ef3-9f34ba074cf4 |
institution | University of Oxford |
language | English |
last_indexed | 2024-03-07T05:48:13Z |
publishDate | 2005 |
publisher | Wiley-Blackwell |
record_format | dspace |
spelling | oxford-uuid:e7f2ab3e-3f5b-4207-9ef3-9f34ba074cf42022-03-27T10:42:55ZEnergy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffractionJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:e7f2ab3e-3f5b-4207-9ef3-9f34ba074cf4Engineering and allied sciencesEnglishSymplectic Elements at OxfordWiley-Blackwell2005Liu, JKim, KGolshan, MLaundy, DKorsunsky, APrecise channel-to-energy conversion is very important in full-pattern refinement in energy-dispersive X-ray diffraction. Careful examination shows that the channel-to-energy conversion is not entirely linear, which presents an obstacle to obtaining accurate quantitative data for lattice strains by pattern refinement. In order to establish an accurate quadratic channel-to-energy conversion function, a Matlab program was written to find the best quadratic coefficient and hence the whole energy conversion function. Then this energy conversion function was used to perform a whole-pattern fitting of the energy-dispersive X-ray diffraction pattern of a Ti64 sample. The strain across the Ti64 bar calculated from the fitting results has been compared with values obtained by single-wavelength X-ray diffraction utilizing a Laue monochromator. © 2005 International Union of Crystallography. |
spellingShingle | Engineering and allied sciences Liu, J Kim, K Golshan, M Laundy, D Korsunsky, A Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction |
title | Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction |
title_full | Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction |
title_fullStr | Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction |
title_full_unstemmed | Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction |
title_short | Energy calibration and full-pattern refinement for strain analysis using energy-dispersive and monochromatic X-ray diffraction |
title_sort | energy calibration and full pattern refinement for strain analysis using energy dispersive and monochromatic x ray diffraction |
topic | Engineering and allied sciences |
work_keys_str_mv | AT liuj energycalibrationandfullpatternrefinementforstrainanalysisusingenergydispersiveandmonochromaticxraydiffraction AT kimk energycalibrationandfullpatternrefinementforstrainanalysisusingenergydispersiveandmonochromaticxraydiffraction AT golshanm energycalibrationandfullpatternrefinementforstrainanalysisusingenergydispersiveandmonochromaticxraydiffraction AT laundyd energycalibrationandfullpatternrefinementforstrainanalysisusingenergydispersiveandmonochromaticxraydiffraction AT korsunskya energycalibrationandfullpatternrefinementforstrainanalysisusingenergydispersiveandmonochromaticxraydiffraction |