Complete (1)H resonance assignment of beta-maltose from (1)H-(1)H DQ-SQ CRAMPS and (1)H (DQ-DUMBO)-(13)C SQ refocused INEPT 2D solid-state NMR spectra and first principles GIPAW calculations.

Complete (1)H resonance assignment of beta-maltose from (1)H-(1)H DQ-SQ CRAMPS and (1)H (DQ-DUMBO)-(13)C SQ refocused INEPT 2D solid-state NMR spectra and first principles GIPAW calculations.

A disaccharide is a challenging case for high-resolution (1)H solid-state NMR because of the 24 distinct protons (14 aliphatic and 10 OH) having (1)H chemical shifts that all fall within a narrow range of approximately 3 to 7 ppm. High-resolution (1)H (500 MHz) double-quantum (DQ) combined rotation...

وصف كامل

التفاصيل البيبلوغرافية
المؤلفون الرئيسيون: Webber, A, Elena, B, Griffin, J, Yates, JR, Pham, T, Mauri, F, Pickard, C, Gil, A, Stein, R, Lesage, A, Emsley, L, Brown, S
التنسيق: Journal article
اللغة:English
منشور في: 2010

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