Measuring fracture toughness of coatings using FIB-machined microbeams

Measuring the toughness of brittle coatings has always been a difficult task. Coatings are often too thin to easily prepare a freestanding sample of a defined geometry to use standard toughness measuring techniques. Using standard indentation techniques gives results influenced by the effect of the...

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Bibliographic Details
Main Authors: Roberts, S, Di Maio, D
Format: Journal article
Language:English
Published: Cambridge University Press 2005
Description
Summary:Measuring the toughness of brittle coatings has always been a difficult task. Coatings are often too thin to easily prepare a freestanding sample of a defined geometry to use standard toughness measuring techniques. Using standard indentation techniques gives results influenced by the effect of the substrate. A new technique for measuring the toughness of coatings is described here. A precracked micro-beam was produced using focused ion beam (FIB) machining, then imaged and loaded to fracture using a nanoindenter. © 2005 Materials Research Society.