$Simultaneous differential scanning calorimetry - synchrotron X-ray powder diffraction: A powerful technique for physical form characterisation in pharmaceutical materials.$

Simultaneous differential scanning calorimetry - synchrotron X-ray powder diffraction: A powerful technique for physical form characterisation in pharmaceutical materials.

We report a powerful new technique: hyphenating synchrotron X-ray powder diffraction (XRD) with differential scanning calorimetry (DSC). This is achieved with a simple modification to a standard laboratory DSC instrument, in contrast to previous reports which have involved extensive and complex modi...

Mô tả đầy đủ

Chi tiết về thư mục
Những tác giả chính:	Clout, A, Buanz, A, Prior, T, Reinhard, C, Wu, Y, O'Hare, D, Williams, G, Gaisford, S
Định dạng:	Journal article
Ngôn ngữ:	English
Được phát hành:	American Chemical Society 2016

Những quyển sách tương tự

Exploring high-throughput synchrotron X-Ray powder diffraction for the structural analysis of pharmaceuticals
Bằng: M. Reinle-Schmitt, et al.
Được phát hành: (2023-12-01)

Simultaneous X-ray Diffraction-Differential Scanning Calorimetry and Physicochemical Characterizations of Spray Dried Drugs and Chitosan Microspheres
Bằng: Kampanart HUANBUTTA, et al.
Được phát hành: (2015-09-01)

Differential Scanning Calorimetry (DSC) and Synchrotron X-ray Diffraction Study of Unmilled and Milled LiBH4: A Partial Release of Hydrogen at Moderate Temperatures
Bằng: J. Huot, et al.
Được phát hành: (2011-12-01)

X-ray characterisation by energy-resolved powder diffraction
Bằng: Hooker, S, et al.
Được phát hành: (2016)

Regeneration of sodium alanate studied by powder in situ neutron and synchrotron X-ray diffraction
Bằng: Humphries, T, et al.
Được phát hành: (2014)

Open-framework fluorinated gallium and aluminium phosphates: an in situ study of the hydrothermal synthesis by X-ray diffraction using synchrotron radiation
Bằng: Loiseau, T, et al.
Được phát hành: (2000)

Morphological Investigation into Starch Bio-Nanocomposites via Synchrotron Radiation and Differential Scanning Calorimetry
Bằng: Huihua Liu, et al.
Được phát hành: (2011-01-01)

Physical Ageing of Amorphous Indapamide Characterised by Differential Scanning Calorimetry
Bằng: Agata Drogoń, et al.
Được phát hành: (2020-08-01)

Time-resolved in situ powder X-ray diffraction reveals the mechanisms of molten salt synthesis
Bằng: Moorhouse, S, et al.
Được phát hành: (2016)

X-Ray powder diffraction. The practical application of the method in the pharmaceutical expertise
Bằng: V. S. Kuzmin, et al.
Được phát hành: (2018-02-01)

Texture analysis in cubic phase polycrystals by single exposure synchrotron X-ray diffraction
Bằng: Xie, M, et al.
Được phát hành: (2013)

Watching solids crystallise using in situ powder diffraction
Bằng: Walton, R, et al.
Được phát hành: (2000)

Watching solids crystallise using in situ powder diffraction
Bằng: Walton, R, et al.
Được phát hành: (2000)

Time-resolved in situ X-ray powder diffraction study of the formation of mesoporous silicates
Bằng: O'Brien, S, et al.
Được phát hành: (1999)

The contribution of synchrotron X-ray powder diffraction to modern zeolite applications: A mini-review and prospects
Bằng: Lo, BTW, et al.
Được phát hành: (2018)

Synchrotron X-ray powder diffraction under high pressures up to 33 MPa for mechanoresponsive materials
Bằng: Hidetaka Kasai, et al.
Được phát hành: (2023-05-01)

Synchrotron X-ray characterisation of crack strain fields in polygranular graphite
Bằng: Barhli, S, et al.
Được phát hành: (2017)

The role of differential scanning calorimetry and x-ray diffraction in identifying crystal continuity in highly oriented samples of die-drawn polypropylene /
Bằng: 260549 Taraiya, A. K., et al.

Kinetic study of the intercalation of cobaltocene by layered metal dichalcogenides with time-resolved in situ X-ray powder diffraction
Bằng: Evans, J, et al.
Được phát hành: (1998)

Determination of the kinetics of crystallisation of gibbsite using time resolved in situ energy dispersive powder X-ray diffraction
Bằng: Fogg, A, et al.
Được phát hành: (2000)

Evaluation of the molecular poisoning phenomenon of W sites in ZSM-5 via synchrotron X-ray powder diffraction
Bằng: Ye, L, et al.
Được phát hành: (2018)

Mineralogy of the Mudeungsan Tuff (Republic of Korea) Using Synchrotron X-ray Powder Diffraction and Rietveld Quantitative Analysis
Bằng: Donghoon Seoung, et al.
Được phát hành: (2021-11-01)

Crystal structure of pentasodium hydrogen dicitrate from synchrotron X-ray powder diffraction data and DFT comparison
Bằng: Alagappa Rammohan, et al.
Được phát hành: (2017-02-01)

Strain analysis in composites using synchrotron X-ray diffraction
Bằng: Wells, K, et al.
Được phát hành: (1998)

Feasibility study of synchrotron x-ray diffraction and absorption spectroscopy for the characterisation of NMC oxides for Li-ion battery cathodes
Bằng: Kim, T, et al.
Được phát hành: (2013)

Mechanistic and kinetic studies of guest ion intercalation into layered double hydroxides using time-resolved, in-situ x-ray powder diffraction
Bằng: Gareth, R, et al.
Được phát hành: (2006)

Structural Characterization of Pharmaceutical Cocrystals with the Use of Laboratory X-ray Powder Diffraction Patterns
Bằng: Vladimir V. Chernyshev
Được phát hành: (2023-04-01)

A new white beam powder diffraction facility at the Daresbury Laboratory synchrotron radiation source
Bằng: Clark, S, et al.
Được phát hành: (1996)

The DIAD Approach to Correlative Synchrotron X‑ray Imaging and Diffraction Analysis of Human Enamel
Bằng: Cyril Besnard, et al.
Được phát hành: (2024-03-01)

Hierarchical modelling of elastic behaviour of human enamel based on synchrotron diffraction characterisation
Bằng: Sui, T, et al.
Được phát hành: (2013)

Hierarchical modelling of elastic behaviour of human enamel based on synchrotron diffraction characterisation.
Bằng: Sui, T, et al.
Được phát hành: (2013)

Spatial differentiation of Brønsted acid sites by probe molecule in zeolite USY using synchrotron X-ray powder diffraction.
Bằng: Ye, L, et al.
Được phát hành: (2017)

Monitoring the methanol conversion process in H-ZSM-5 using synchrotron X-ray powder diffraction-mass spectrometry
Bằng: Lo, BTW, et al.
Được phát hành: (2018)

Elucidation of adsorbate structures and interactions on Brønsted acid sites in H‐ZSM‐5 by synchrotron X‐ray powder diffraction
Bằng: Lo, B, et al.
Được phát hành: (2016)

Synthesis and Characterization of a Monoclinic Crystalline Phase of Hydroxyapatite by Synchrotron X-ray Powder Diffraction and Piezoresponse Force Microscopy
Bằng: Ricardo Pérez-Solis, et al.
Được phát hành: (2018-12-01)

Direct Detection of Bound Water in Hydrated Powders of Lysozyme by Differential Scanning Calorimetry
Bằng: Judith Peters, et al.
Được phát hành: (2024-09-01)

Advanced strain analysis by high energy synchrotron X-ray diffraction
Bằng: Korsunsky, A, et al.
Được phát hành: (2002)

A synchrotron X-ray diffraction study of in situ biaxial deformation
Bằng: Collins, D, et al.
Được phát hành: (2015)

Advanced strain analysis by high energy synchrotron X-ray diffraction
Bằng: Korsunsky, A, et al.
Được phát hành: (2002)

Probing the deformation of ductile polycrystals by synchrotron x-ray micro-diffraction
Bằng: Hofmann, F, et al.
Được phát hành: (2011)