A spectrometer designed for 6.7 and 14.1 T DNP-enhanced solid-state MAS NMR using quasi-optical microwave transmission.

A spectrometer designed for 6.7 and 14.1 T DNP-enhanced solid-state MAS NMR using quasi-optical microwave transmission.

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A Dynamic Nuclear Polarisation (DNP) enhanced solid-state Magic Angle Spinning (MAS) NMR spectrometer operating at 6.7 T is described and demonstrated. The 187 GHz TE(13) fundamental mode of the FU CW VII gyrotron is used as the microwave source for this magnetic field strength and 284 MHz (1)H DNP-...

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Bibliographic Details
Main Authors: Pike, K, Kemp, T, Takahashi, H, Day, R, Howes, A, Kryukov, E, MacDonald, J, Collis, A, Bolton, DR, Wylde, R, Orwick, M, Kosuga, K, Clark, A, Idehara, T, Watts, A, Smith, G, Newton, M, Dupree, R, Smith, M
Format: Journal article
Language:English
Published: 2012

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