Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid
Magnetic nanoparticles ( MNPs) coated polyaniline (P ANI) was successfully synthesized and further used for removal of 2.4-dinitrophenol. The presence of PANI coatings on the surface of MNPs was confirmed by using Fourier Transform Infrared (FT-IR) Spectroscopy. Scanning Electron Microscopy (SEM) a...
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| Format: | Student Project |
| Language: | English |
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Faculty of Applied Sciences
2017
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| Online Access: | https://ir.uitm.edu.my/id/eprint/25362/1/PPb_SHUHAILI%20RASHID%20AS%20N%2017_5.pdf |
| _version_ | 1796902098829312000 |
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| author | Rashid, Shuhaili |
| author_facet | Rashid, Shuhaili |
| author_sort | Rashid, Shuhaili |
| collection | UITM |
| description | Magnetic nanoparticles ( MNPs) coated polyaniline (P ANI) was successfully synthesized and further used for removal of 2.4-dinitrophenol. The presence of PANI coatings on the surface of MNPs was confirmed by using Fourier Transform
Infrared (FT-IR) Spectroscopy. Scanning Electron Microscopy (SEM) and X-ray Diffractometry (XRD) analysis. MNPs coated PANI (MNPs/PANI) showed higher capabilities to remove 2,4- dinitrophenol (2.4-DNP) via spectrophotometry at 358 nm by using Ultraviolet Visible (UV-Vis) Spectrophotometer. Different parameters
such as pH, contact time, initial concentration and temperature, amount of adsorbent, interfering ions were investigated to optimize the performance of MNPs/P ANI in removal of 2,4-DNP. In addition, the reusabilities of MNPs/P ANI was also studied to add up its economic value. The best perfonnance of
MNPs/P ANI to remove 2,4-DNP molecules was found at pH 7, I 05 minutes contact time, IO ppm initial concentration of 2,4-DNP with 298.15 K temperature and I 0 mg of adsorbent amount. The percentage removal (¾R) of 2,4-DNP was still up to 90% in the presence of chloride (Cl-) ions, nitrate (NO3-) ions and sulfate (SO42-)
ions. Lastly MNPs/P ANI was used up to five cycles. |
| first_indexed | 2024-03-06T01:59:50Z |
| format | Student Project |
| id | uitm.eprints-5362 |
| institution | Universiti Teknologi MARA |
| language | English |
| last_indexed | 2024-03-06T01:59:50Z |
| publishDate | 2017 |
| publisher | Faculty of Applied Sciences |
| record_format | dspace |
| spelling | uitm.eprints-53622019-09-11T02:32:31Z https://ir.uitm.edu.my/id/eprint/25362/ Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid Rashid, Shuhaili QD Chemistry Oxidation Magnetic nanoparticles ( MNPs) coated polyaniline (P ANI) was successfully synthesized and further used for removal of 2.4-dinitrophenol. The presence of PANI coatings on the surface of MNPs was confirmed by using Fourier Transform Infrared (FT-IR) Spectroscopy. Scanning Electron Microscopy (SEM) and X-ray Diffractometry (XRD) analysis. MNPs coated PANI (MNPs/PANI) showed higher capabilities to remove 2,4- dinitrophenol (2.4-DNP) via spectrophotometry at 358 nm by using Ultraviolet Visible (UV-Vis) Spectrophotometer. Different parameters such as pH, contact time, initial concentration and temperature, amount of adsorbent, interfering ions were investigated to optimize the performance of MNPs/P ANI in removal of 2,4-DNP. In addition, the reusabilities of MNPs/P ANI was also studied to add up its economic value. The best perfonnance of MNPs/P ANI to remove 2,4-DNP molecules was found at pH 7, I 05 minutes contact time, IO ppm initial concentration of 2,4-DNP with 298.15 K temperature and I 0 mg of adsorbent amount. The percentage removal (¾R) of 2,4-DNP was still up to 90% in the presence of chloride (Cl-) ions, nitrate (NO3-) ions and sulfate (SO42-) ions. Lastly MNPs/P ANI was used up to five cycles. Faculty of Applied Sciences 2017 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/25362/1/PPb_SHUHAILI%20RASHID%20AS%20N%2017_5.pdf Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid. (2017) [Student Project] (Unpublished) |
| spellingShingle | QD Chemistry Oxidation Rashid, Shuhaili Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title | Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_full | Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_fullStr | Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_full_unstemmed | Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_short | Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_sort | synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2 4 dinitrophenol shuhaili rashid |
| topic | QD Chemistry Oxidation |
| url | https://ir.uitm.edu.my/id/eprint/25362/1/PPb_SHUHAILI%20RASHID%20AS%20N%2017_5.pdf |
| work_keys_str_mv | AT rashidshuhaili synthesisandcharacterizationofmagneticnanoparticlescoatedwithpolyanilineforremovalof24dinitrophenolshuhailirashid |