Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract

Cinnamon is a spice obtained from the inner bark of cinnamomum tree. Cinnamaldehyde, the major consitituent of the cinnamon essential oil is responsible for the flavor and aroma of whole cinnamon. Cinnamaldehyde have various medicinal application including neuroprotection. Thus, this study intends...

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Main Authors: Zetty Shafiqa Othman, Mohamad Yusof Maskat, Nur Hasyareeda Hassan
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2020
Online Access:http://journalarticle.ukm.my/15390/1/4.pdf
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author Zetty Shafiqa Othman,
Mohamad Yusof Maskat,
Nur Hasyareeda Hassan,
author_facet Zetty Shafiqa Othman,
Mohamad Yusof Maskat,
Nur Hasyareeda Hassan,
author_sort Zetty Shafiqa Othman,
collection UKM
description Cinnamon is a spice obtained from the inner bark of cinnamomum tree. Cinnamaldehyde, the major consitituent of the cinnamon essential oil is responsible for the flavor and aroma of whole cinnamon. Cinnamaldehyde have various medicinal application including neuroprotection. Thus, this study intends to identify the optimal condition for cinnamaldehyde extraction with high antioxidant activity of cinnamon extract. Responses (cinnamaldehyde yield, TPC, and TEAC) were optimized using response surface methodology (RSM) by employing two factors (temperature and extraction time) based on a three level face centered central composite design (CCD). Level of extraction temperature used were 30 °C, 55 °C and 80 °C, while extraction time were 4, 7, and 10 h. The CCD consisted of 8 experimental point and 5 replicates of central points. The optimal conditions to obtain maximum cinnamaldehyde yield, TPC and TEAC were extraction temperature of 37 °C at 5 h extraction time with predicted cinnamaldehyde yield of 3.05 mg/g, TPC of 682.17 mg GAE/ g and TEAC of 821.57 µmol TE/g respectively. The experimental values obtained for the cinnamaldehyde yield, TPC, and TEAC under the optimal condition were 3.11 ± 0.71 mg/g, 682.66 ± 54.85 mg GAE/g, and 817.89 ± 9.03 µmol TE/g. The proximity between experimental and prediction values verify the fitness of RSM models applied for determination of optimal condition for cinnamaldehyde extraction.
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spelling ukm.eprints-153902020-10-23T00:45:58Z http://journalarticle.ukm.my/15390/ Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract Zetty Shafiqa Othman, Mohamad Yusof Maskat, Nur Hasyareeda Hassan, Cinnamon is a spice obtained from the inner bark of cinnamomum tree. Cinnamaldehyde, the major consitituent of the cinnamon essential oil is responsible for the flavor and aroma of whole cinnamon. Cinnamaldehyde have various medicinal application including neuroprotection. Thus, this study intends to identify the optimal condition for cinnamaldehyde extraction with high antioxidant activity of cinnamon extract. Responses (cinnamaldehyde yield, TPC, and TEAC) were optimized using response surface methodology (RSM) by employing two factors (temperature and extraction time) based on a three level face centered central composite design (CCD). Level of extraction temperature used were 30 °C, 55 °C and 80 °C, while extraction time were 4, 7, and 10 h. The CCD consisted of 8 experimental point and 5 replicates of central points. The optimal conditions to obtain maximum cinnamaldehyde yield, TPC and TEAC were extraction temperature of 37 °C at 5 h extraction time with predicted cinnamaldehyde yield of 3.05 mg/g, TPC of 682.17 mg GAE/ g and TEAC of 821.57 µmol TE/g respectively. The experimental values obtained for the cinnamaldehyde yield, TPC, and TEAC under the optimal condition were 3.11 ± 0.71 mg/g, 682.66 ± 54.85 mg GAE/g, and 817.89 ± 9.03 µmol TE/g. The proximity between experimental and prediction values verify the fitness of RSM models applied for determination of optimal condition for cinnamaldehyde extraction. Penerbit Universiti Kebangsaan Malaysia 2020-05 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/15390/1/4.pdf Zetty Shafiqa Othman, and Mohamad Yusof Maskat, and Nur Hasyareeda Hassan, (2020) Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract. Sains Malaysiana, 49 (5). pp. 995-1002. ISSN 0126-6039 http://www.ukm.my/jsm/malay_journals/jilid49bil5_2020/KandunganJilid49Bil5_2020.html
spellingShingle Zetty Shafiqa Othman,
Mohamad Yusof Maskat,
Nur Hasyareeda Hassan,
Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract
title Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract
title_full Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract
title_fullStr Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract
title_full_unstemmed Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract
title_short Optimization of cinnamaldehyde extraction and antioxidant activity of Ceylon cinnamon extract
title_sort optimization of cinnamaldehyde extraction and antioxidant activity of ceylon cinnamon extract
url http://journalarticle.ukm.my/15390/1/4.pdf
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