Characterization of titanium alloy-hydroxyapatite composite through powder injection molding

Powder injection moulding (PIM) is a process that combines the technologies of plastic injection moulding and powder metallurgy. The fabrication of titanium alloy-hydroxyapatite (Ti6Al4V/HA) composite using PIM is still poorly reported due to the difficulties in processing two different material...

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Main Authors: Mohd Ikram Ramli, Farhana Mohd Foudzi, Abu Bakar Sulong, Fatin Aqilah Abdul Yazid, Norhamidi Muhamad, Hui, David
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2020
Online Access:http://journalarticle.ukm.my/17215/1/25.pdf
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author Mohd Ikram Ramli,
Farhana Mohd Foudzi,
Abu Bakar Sulong,
Fatin Aqilah Abdul Yazid,
Norhamidi Muhamad,
Hui, David
author_facet Mohd Ikram Ramli,
Farhana Mohd Foudzi,
Abu Bakar Sulong,
Fatin Aqilah Abdul Yazid,
Norhamidi Muhamad,
Hui, David
author_sort Mohd Ikram Ramli,
collection UKM
description Powder injection moulding (PIM) is a process that combines the technologies of plastic injection moulding and powder metallurgy. The fabrication of titanium alloy-hydroxyapatite (Ti6Al4V/HA) composite using PIM is still poorly reported due to the difficulties in processing two different materials namely the metal and ceramic. Such promising composite can be proposed as an implant material due to its great properties. Hence, this work aims to characterise the properties of Ti6Al4V/HA composite produced by PIM. In this work, 90 wt% of Ti6Al4V and 10 wt% of HA were mixed with a binder system of 60 wt% palm stearin and 40 wt% polyethylene. The powder loading of the feedstock was 66 vol%. The feedstock with a pseudoplastic flow is preferred in PIM as fewer defects are formed during the injection moulding process. Moreover, the binders are removed in two stages namely the solvent and thermal debinding. Based on the observation, the removal of palm stearin created capillary routes that help to remove polyethylene during thermal debinding. Next, sintering was performed at three different temperatures, which include 1100o C, 1200o C and 1300o C. The heating rate, holding time and cooling rate was set at 3o C/min, 90 min and 6o C/min, respectively. It was found that Ti6Al4V/HA sintered at 1300o C yielded the highest density of 4.13 g/cm3 . In addition, such sintered part also generated the highest flexural and Young’s modulus with the values of 86.4 MPa and 15.04 GPa, respectively. These values are approximately in the range of the physical and mechanical properties of the extant bone-implant.
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spelling ukm.eprints-172152021-07-27T02:59:06Z http://journalarticle.ukm.my/17215/ Characterization of titanium alloy-hydroxyapatite composite through powder injection molding Mohd Ikram Ramli, Farhana Mohd Foudzi, Abu Bakar Sulong, Fatin Aqilah Abdul Yazid, Norhamidi Muhamad, Hui, David Powder injection moulding (PIM) is a process that combines the technologies of plastic injection moulding and powder metallurgy. The fabrication of titanium alloy-hydroxyapatite (Ti6Al4V/HA) composite using PIM is still poorly reported due to the difficulties in processing two different materials namely the metal and ceramic. Such promising composite can be proposed as an implant material due to its great properties. Hence, this work aims to characterise the properties of Ti6Al4V/HA composite produced by PIM. In this work, 90 wt% of Ti6Al4V and 10 wt% of HA were mixed with a binder system of 60 wt% palm stearin and 40 wt% polyethylene. The powder loading of the feedstock was 66 vol%. The feedstock with a pseudoplastic flow is preferred in PIM as fewer defects are formed during the injection moulding process. Moreover, the binders are removed in two stages namely the solvent and thermal debinding. Based on the observation, the removal of palm stearin created capillary routes that help to remove polyethylene during thermal debinding. Next, sintering was performed at three different temperatures, which include 1100o C, 1200o C and 1300o C. The heating rate, holding time and cooling rate was set at 3o C/min, 90 min and 6o C/min, respectively. It was found that Ti6Al4V/HA sintered at 1300o C yielded the highest density of 4.13 g/cm3 . In addition, such sintered part also generated the highest flexural and Young’s modulus with the values of 86.4 MPa and 15.04 GPa, respectively. These values are approximately in the range of the physical and mechanical properties of the extant bone-implant. Penerbit Universiti Kebangsaan Malaysia 2020 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/17215/1/25.pdf Mohd Ikram Ramli, and Farhana Mohd Foudzi, and Abu Bakar Sulong, and Fatin Aqilah Abdul Yazid, and Norhamidi Muhamad, and Hui, David (2020) Characterization of titanium alloy-hydroxyapatite composite through powder injection molding. Jurnal Kejuruteraan, 32 (4). pp. 735-742. ISSN 0128-0198 https://www.ukm.my/jkukm/volume-324-2020/
spellingShingle Mohd Ikram Ramli,
Farhana Mohd Foudzi,
Abu Bakar Sulong,
Fatin Aqilah Abdul Yazid,
Norhamidi Muhamad,
Hui, David
Characterization of titanium alloy-hydroxyapatite composite through powder injection molding
title Characterization of titanium alloy-hydroxyapatite composite through powder injection molding
title_full Characterization of titanium alloy-hydroxyapatite composite through powder injection molding
title_fullStr Characterization of titanium alloy-hydroxyapatite composite through powder injection molding
title_full_unstemmed Characterization of titanium alloy-hydroxyapatite composite through powder injection molding
title_short Characterization of titanium alloy-hydroxyapatite composite through powder injection molding
title_sort characterization of titanium alloy hydroxyapatite composite through powder injection molding
url http://journalarticle.ukm.my/17215/1/25.pdf
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